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STUDY ON PROPERTY PREDICTION FOR SEALING ALLOYS

Z.N. Xia , S.G. Lai , Y.Z.Sun and Y.W. Lu(Department of Materials Science and Engineering , Tsinghua University , Beijing 100084 , ChinaManuscript received 4 March 1996)

金属学报(英文版)

This paper describes a model of property prediction for alloys using the mapping function and self-learning ability of artificial neural network. By learning from experimental data, the neural network induces the relationship between composition, processing and properties of alloys, and predicts the properties with given composition and processing parameters of new alloys.The verification of sealing alloys demonstrates that the artificial neural network is an effective method for materials design and properties prediction.

关键词: :property prediction , null , null

Service Performance of Engineering Materials

Andrej Atrens

材料科学技术(英文)

Corrosion research by Atrens and co-workers has made significant contributions to the understanding of the service performance of engineering materials. This includes: (1) elucidated corrosion mechanisms of Mg alloys, stainless steels and Cu alloys, (2) developed an improved understanding of passivity in stainless steels and binary alloys such as Fe-Cr, Ni-Cr, Co-Cr, Fe-Ti, and Fe-Si, (3) developed an improved understanding of the melt spinning of Cu alloys, and (4) elucidated mechanisms of environment assisted fracture (EAF) of steels and Zr alloys. This paper summarises contributions in the following: (1) intergranular stress corrosion cracking of pipeline steels, (2) atmospheric corrosion and patination of Cu, (3) corrosion of Mg alloys, and (4) transgranular stress corrosion cracking of rock bolts.

关键词: Stress corrosion cracking , null , null

Stereology in Materials Science

LIU Guoquan Department of Materials Science and Engineering , University of Science and Technology Beijing , 100083 , China.

材料科学技术(英文)

Quantitative analysis of populations having a geometric structure,which has developed into a special scientific subject called microstructology or stereology,is of great importance to the characterization and evaluation of microstructures and their evolution in various processes.This paper, besides a brief discussion on those topics such as the recent developments of computer assisted image analysis,mathematical morphology,and fractal analysis,will mainly focus on the scope,fundamen- tals,present status,and perspectives of classical stereology.Several case examples of its application to materials science will also be given.

关键词: stereology , null , null , null

Yb0.005Y0.708Lu0.287VO4混晶的生长和材料性质

张炳涛 , 滕冰 , 钟德高 , 曹丽凤 , 李建宏 ,

人工晶体学报

采用提拉法生长出Ybb0.005Y0.708Lu0.287VO4晶体.在室温下,对Yb0.005Y0.708Lu0.287VO4晶体进行了XRPD测试,计算了晶格常数(a=b=0.7091 nm,c=0.6273 nm)和密度(4.826 g/cm3).对混晶的(100)面进行了腐蚀,腐蚀坑呈四棱锥形状.平均线膨胀系数α1=1.285×10-6 K-1,α3=7.030 ×10-6 K-1,温度在330.15 K和570.15 K之间变化时,比热为0.494 ~0.617 J/g·K.

关键词: 钒酸盐晶体 , 腐蚀坑 , 膨胀系数 , 比热 , 热导率

Biomimicry of bamboo bast fiber with engineering composite materials

Materials Science & Engineering C-Biomimetic Materials Sensors and Systems

Bamboo, one of the strongest natural structural composite materials, has many distinguishing features. It has been found that its reinforcement unit, hollow, multilayered and spirally-wound bast fiber, plays an extremely important role in its mechanical behavior. In the present work, on the basis of the study on bamboo bast fiber and wood tracheid, a biomimetic model of the reinforcing element, composed of two layers of helically wound fiber, was suggested. To detect the structural characteristics of such a microstructure, four types of macro fiber specimens made of engineering composites were employed: axially aligned solid and hollow cylinders, and single- and double-helical hollow cylinders. These specimens were subjected to several possible loadings, and the experimental results reveal that only the double-helical structural unit possesses the optimum comprehensive mechanical properties. An interlaminar transition zone model imitating bamboo bast fiber was proposed and was verified by engineering composite materials. In our work, the transition zone can increase the interlaminar shear strength of the composite materials by about 15%. These biomimetic structural models can be applied in the design and manufacture of engineering composite materials.

关键词: bamboo;bast fiber;biomimetics;engineering composites

Y3+掺杂Ce∶Li6Lu(BO3)3闪烁体的发光性能研究

孙丹丹 , 潘尚可 , 任国浩 , 吴云涛 , 商珊珊 , 张国庆

无机材料学报 doi:10.3724/SP.J.1077.2013.12735

针对Ce:Li6Lu(BO3)3晶体有效原子序数(zeff)高的问题,采用低原子序数的Y3+离子部分置换晶体中的Lu3+离子.通过固相合成法制备了Ce:Li6Lu1-xYx(BO3)3(0≤x≤1)固溶体.X射线粉末衍射(XRD)分析表明,该系列固溶体结构与Li6Gd(BO3)3晶体相同,空间群为P21/c.其X射线激发发射(XSL)的发光强度随着Y3+的含量增加而降低,当x=0.5时,固溶体的有效原子序数与Li6Gd(BO3)3闪烁体相当,但XSL发光强度是其1.4倍.Ce:Li6Lu0.5Y0.5(BO3)3的XSL光谱和PL光谱都在400 nm附近出现Ce3+离子的特征峰,可拟合出361和419 nm两个发光分量,分别对应于Ce3+离子的激发态电子的5d1→2F5/2和5d1→2F7/2能级跃迁.Ce:Li6Lu0.5Y0.5(BO3)3固溶体的衰减时间比Ce:Li6Lu(BO3)3略长,为19.6 ns.当x=0.50~0.70时,Ce:Li6Lu1-xYx(BO3)3(0≤x≤1)闪烁体比较适合作为中子探测材料.

关键词: 固相合成 , Ce∶Li6LU1-xYx(BO3)3 , X射线激发发射谱 , PL光谱 , 衰减时间

LuxY1-xAl 3:Ce晶体中伴生(Lu,Y3 Al5O12:Ce相成因研究

丁栋舟 , 陆晟 , 潘尚可 , 张卫东 , 王广东 , 任国浩

无机材料学报 doi:10.3724/SP.J.1077.2008.00434

采用提拉法制备了LuxY1-xAlO3:Ce晶体样品, 通过XRD物相分析和成分分析, 并结合Lu2O 3-Al2O3二元体系相图以及LuxY1-x AlO3:Ce结构稳定性方面的分析与讨论, 结果表明: 随着熔体中Lu元素含量的增加, 熔体分层加剧, 析晶LuxY1-xAlO3:Ce相的熔体组成区间将向富Lu一侧偏移, 这使得晶体上部易伴生(Lu,Y)3Al5O12:Ce相; 而随着Lu元素含量的提高, LuxY1-xAlO3:Ce晶体的热稳定性降低, 氧空位的存在则使晶体的热稳定性进一步降低, 在接种过程中籽晶表面易发生相分解反应生成(Lu,Y)3 Al5O12:Ce和(Lu,Y) 4 Al2O9:Ce, 籽晶表面相分解产物(Lu,Y)3Al5O12:Ce提供了诱导析晶(Lu,Y)3Al5O12 :Ce相所需的晶核, 这使得晶体的外
表面处易伴生(Lu,Y)3Al5O12:Ce相. 调整配料组成使 n(Lu,Y)2O3 ): n (Al2O3)=1.17~1.00, 加大熔体内部和固液界面处的温度梯度以改善熔体对流、抑制熔体分层以及籽晶表面处的相分解等有助于高Lu元素含量LuxY1-xAlO3 :Ce晶体的获得.

关键词: 铝酸钇镥晶体 , perovskite , garnet , accompany

LuxY1-xAlO3:Ce晶体中伴生(Lu,Y)3Al5O12:Ce相成因研究

丁栋舟 , 陆晟 , 潘尚可 , 张卫东 , 王广东 , 任国浩

无机材料学报 doi:10.3321/j.issn:1000-324X.2008.03.004

采用提拉法制备了LuxY1-xAlOa:Ce晶体样品,通过XRD物相分析和成分分析,并结合Lu2O3-Al2O3二元体系相图以及LuxY1-xAlO3:Ce 结构稳定性方面的分析与讨论,结果表明:随着熔体中Lu元素含量的增加,熔体分层加剧,析晶LuxY1-xAlO3:Ce相的熔体组成区间将向富Lu一侧偏移,这使得晶体上部易伴生(Lu,Y)3Al5O12:Ce相;而随着Lu元素含量的提高, LuxY1-xAlO3:Ce晶体的热稳定性降低,氧空位的存在则使晶体的热稳定性进一步降低,在接种过程中籽晶表面易发生相分解反应生成(Lu,Y)3Al5O12:Ce和(Lu,Y)4Al2O9:Ce,籽晶表面相分解产物(Lu,Y)3Al5O12:Ce提供了诱导析晶(Lu,Y)3Al5O12:Ce相所需的晶核,这使得晶体的外表面处易伴生(Lu,Y)3Al5O12:Ce相.调整配料组成使n((Lu,Y)2O3):n(A12O3)=1.17~100,加大熔体内部和固液界面处的温度梯度以改善熔体对流、抑制熔体分层以及籽晶表面处的相分解等有助于高Lu元素含量LuxY1-xAlO3:Ce晶体的获得.

关键词: 铝酸钇镥晶体 , 钙钛矿 , 石榴石 , 伴生

超细(W,Ni,Fe,Y)复合粉末制备过程中稀土Y的物相形态变化

彭石高 , 丁飞 ,

中国有色金属学报

采用溶胶-喷雾干燥-氢还原法制备稀土Y含量分别为0,0.4%,5%,10%和20%的超细(W,Ni,Fe,Y)复合粉末,采用XRD研究煅烧温度和还原温度以及稀土Y含量变化时复合粉末体在制备过程中的相结构变化规律.结果表明:喷雾干燥前驱体随煅烧温度的升高渐渐从非晶体向复合氧化物晶化转变,添加稀土Y的粉末前驱体经煅烧后,YW形成复合氧化物Y2W3O12,且稀土Y可以有效地抑制粉末颗粒长大;随着Y含量的增加,YW的复合氧化物明显增加,Y2W3O12在700℃才能被还原成低氧复合氧化物相:含5%稀土Y粉末中的Y2W3O12被还原生成新相Y2WO6;当稀土Y增加到10%以上时,不仅生成Y2WO6,还生成另一种新相Y6W2OB15.

关键词: W-Ni-Fe复合粉末 , 纳米粉末 , 稀土 , Y

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