{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"通过力学性能检测、SEM和XRD分析,研究了<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>及固溶处理对AZ31镁合金组织和性能的影响,并分析了其断裂方式。结果表明：稀土<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>能够细化铸态α-Mg基体组织,对镁合金具有较好的细晶强化作用;<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>和铝<span style=\"color:red\">元素</span>形成的Al2Y化合物,在细化晶粒的同时均匀分布于晶界处,可强化晶界,提高合金的力学性能;<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>质量分数为1.0%时,合金的力学性能最佳;进行440℃×10h的固溶处理能使加入0.5%（质量分数）<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>的合金组织最为均匀;加入<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>后,合金以韧性断裂和准解理断裂相结合的方式断裂。","authors":[{"authorName":"李成","id":"d63d27f2-7255-49b3-bc4a-0d0fd37c4f41","originalAuthorName":"李成"},{"authorName":"蔡庆伍","id":"e938eaf8-e1f5-4e7c-ba9e-9986048b456e","originalAuthorName":"蔡庆伍"},{"authorName":"江海涛","id":"9d310d8c-5eb5-4419-96e5-2d6435f813e6","originalAuthorName":"江海涛"},{"authorName":"孟强","id":"6f4d8812-1d70-41df-8cfd-ad47b33e56d0","originalAuthorName":"孟强"},{"authorName":"王哲","id":"126b4bcb-1be2-45b1-aa5b-106d93434b70","originalAuthorName":"王哲"}],"doi":"","fpage":"11","id":"bf3c7e6b-edbb-4646-8e8b-9260b9f11e40","issue":"1","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"9b09d34d-b559-44a7-b0cd-4d856c59d2e6","keyword":"镁合金","originalKeyword":"镁合金"},{"id":"9bac46fc-b968-47ba-9d99-f2bf0b781169","keyword":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>","originalKeyword":"钇元素"},{"id":"0fd8da1a-c4a5-44f6-ba5e-a96d896823f4","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"01c8753c-ce72-47ef-9181-24a16d33adf1","keyword":"固溶处理","originalKeyword":"固溶处理"}],"language":"zh","publisherId":"jxgccl201201003","title":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>及固溶处理对AZ31镁合金组织和性能的影响","volume":"36","year":"2012"},{"abstractinfo":"研究了不同<span style=\"color:red\">钇</span>含量（质量分数为0，0．94％，2．67％，4．61％）对铸态Mg-6Zn-0．7Zr合金显微组织及力学性能的影响。结果表明：<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>主要富集在晶界；晶界析出相呈鱼骨状和块状，并逐渐连续成网状；当<span style=\"color:red\">钇</span>的质量分数为0．94％时，合金主要为α—Mg、Mg7Zn3和Mg3Y2Zn。相；当<span style=\"color:red\">钇</span>的质量分数为2．67％时，析出相为α—Mg、Mg12YZn和Mg3Y2Zn3相；随着<span style=\"color:red\">钇</span>含量的增多，合金的抗拉强度、屈服强度和伸长率先增大后减小，当<span style=\"color:red\">钇</span>的质量分数为2．67％时，合金的性能最佳，抗拉强度和屈服强度分别为250．4，125．3MPa，伸长率为12．73%。","authors":[{"authorName":"宋奇慧","id":"b46cede9-456f-48ef-bc0f-ec2f68eba6f6","originalAuthorName":"宋奇慧"},{"authorName":"王新年","id":"f3fbf829-b350-4f2f-87df-a83ee3292d14","originalAuthorName":"王新年"},{"authorName":"朱兆军","id":"b6208716-8401-48f2-8caa-fdd7b0100b7e","originalAuthorName":"朱兆军"}],"doi":"","fpage":"21","id":"8f633d56-76ad-4c18-997b-5895b58e855f","issue":"7","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"e4972430-1893-404a-9299-785792d29127","keyword":"镁锌锆合金","originalKeyword":"镁锌锆合金"},{"id":"b7158d36-85e2-482d-bddb-2baa714fad66","keyword":"组织","originalKeyword":"组织"},{"id":"49a1aae0-8767-432f-a478-dc2b03a6644b","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"b1381fc9-f440-428a-94e8-ad8048a20b5a","keyword":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>","originalKeyword":"钇元素"}],"language":"zh","publisherId":"jxgccl201207007","title":"<span style=\"color:red\">钇</span>含量对铸态镁锌锆合金组织及力学性能的影响","volume":"36","year":"2012"},{"abstractinfo":"用井式电阻炉制备了不同<span style=\"color:red\">钇</span>含量的Mg-9Al-2.25Sr耐热镁合金,借助OM、SEM、EDS、XRD以及力学性能试验机等研究<span style=\"color:red\">钇</span>含量对合金显微组织和力学性能的影响.结果表明:<span style=\"color:red\">钇</span>可细化试验镁合金的组织,与铝结合生成弥散分布的颗粒状Al2Y高温相,有效抑制了β-Mg17Al12低温相的析出；在<span style=\"color:red\">钇</span>质量分数为0.35％时,合金的晶粒组织细小均匀,综合力学性能最优,其在室温和高温(200℃)下的抗拉强度、屈服强度分别为207.65,159.77MPa和192.52,134.83MPa.","authors":[{"authorName":"张金玲","id":"642450a4-f730-4c0d-bc59-e8c64ecb3699","originalAuthorName":"张金玲"},{"authorName":"刘璐","id":"d0b60e66-37e8-4534-975a-a98d60466153","originalAuthorName":"刘璐"},{"authorName":"王昕","id":"ed76b0d3-67c8-43d6-9c96-2c704fff9097","originalAuthorName":"王昕"},{"authorName":"范晋平","id":"53548554-831a-408c-bd24-285a6d37c8bd","originalAuthorName":"范晋平"},{"authorName":"王社斌","id":"55375f49-44f1-45dc-8cfa-fa9216b4df46","originalAuthorName":"王社斌"}],"doi":"","fpage":"5","id":"157cb63e-774b-4470-95be-58521afb563d","issue":"3","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"00a73f1d-aeca-4f6d-8c4c-82b95f0206d6","keyword":"耐热镁合金","originalKeyword":"耐热镁合金"},{"id":"4d7364ef-1eea-4bd5-9c91-8fd82c41396f","keyword":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>","originalKeyword":"钇元素"},{"id":"f9b9a966-1f7e-4d7a-9162-3acbb5e6ad1c","keyword":"显微组织","originalKeyword":"显微组织"},{"id":"a0027fe8-caa1-45d4-ac62-4f9a998fadeb","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"jxgccl201303002","title":"<span style=\"color:red\">钇</span>含量对Mg-9Al-2.25Sr耐热镁合金组织及力学性能的影响","volume":"37","year":"2013"},{"abstractinfo":"基于现有低碳钢焊条性能的特点,针对典型低碳钢焊条(E4303型焊条)抗裂性较差的问题,在新型低碳钢焊条药皮配方开发研制中采取药皮过渡微量的镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>.通过冲击韧性、拉伸、硬度、金相等试验研究镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>对低碳钢焊条熔敷金属组织和力学性能的影响,利用扫描电子显微镜对显微组织进行观察分析,用X射线荧光光谱仪进行光谱分析.结果表明:加入适量的镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>能够细化熔敷金属显微组织,提高熔敷金属的冲击韧性.当镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>加入量最佳(3.5%镧和0.6%<span style=\"color:red\">钇</span>)时,熔敷金属的冲击韧性提高了38.8%,延伸率提高了25%,抗拉强度提高了11.9%,屈服强度提高了10.9%,硬度却不下降.","authors":[{"authorName":"郭永环","id":"8dd11045-c831-4ba6-abf9-d2344255a291","originalAuthorName":"郭永环"},{"authorName":"范希营","id":"8c452b9b-a8e8-{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"通过力学性能检测、SEM和XRD分析,研究了<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>及固溶处理对AZ31镁合金组织和性能的影响,并分析了其断裂方式。结果表明：稀土<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>能够细化铸态α-Mg基体组织,对镁合金具有较好的细晶强化作用;<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>和铝<span style=\"color:red\">元素</span>形成的Al2Y化合物,在细化晶粒的同时均匀分布于晶界处,可强化晶界,提高合金的力学性能;<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>质量分数为1.0%时,合金的力学性能最佳;进行440℃×10h的固溶处理能使加入0.5%（质量分数）<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>的合金组织最为均匀;加入<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>后,合金以韧性断裂和准解理断裂相结合的方式断裂。","authors":[{"authorName":"李成","id":"d63d27f2-7255-49b3-bc4a-0d0fd37c4f41","originalAuthorName":"李成"},{"authorName":"蔡庆伍","id":"e938eaf8-e1f5-4e7c-ba9e-9986048b456e","originalAuthorName":"蔡庆伍"},{"authorName":"江海涛","id":"9d310d8c-5eb5-4419-96e5-2d6435f813e6","originalAuthorName":"江海涛"},{"authorName":"孟强","id":"6f4d8812-1d70-41df-8cfd-ad47b33e56d0","originalAuthorName":"孟强"},{"authorName":"王哲","id":"126b4bcb-1be2-45b1-aa5b-106d93434b70","originalAuthorName":"王哲"}],"doi":"","fpage":"11","id":"bf3c7e6b-edbb-4646-8e8b-9260b9f11e40","issue":"1","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"9b09d34d-b559-44a7-b0cd-4d856c59d2e6","keyword":"镁合金","originalKeyword":"镁合金"},{"id":"9bac46fc-b968-47ba-9d99-f2bf0b781169","keyword":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>","originalKeyword":"钇元素"},{"id":"0fd8da1a-c4a5-44f6-ba5e-a96d896823f4","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"01c8753c-ce72-47ef-9181-24a16d33adf1","keyword":"固溶处理","originalKeyword":"固溶处理"}],"language":"zh","publisherId":"jxgccl201201003","title":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>及固溶处理对AZ31镁合金组织和性能的影响","volume":"36","year":"2012"},{"abstractinfo":"研究了不同<span style=\"color:red\">钇</span>含量（质量分数为0，0．94％，2．67％，4．61％）对铸态Mg-6Zn-0．7Zr合金显微组织及力学性能的影响。结果表明：<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>主要富集在晶界；晶界析出相呈鱼骨状和块状，并逐渐连续成网状；当<span style=\"color:red\">钇</span>的质量分数为0．94％时，合金主要为α—Mg、Mg7Zn3和Mg3Y2Zn。相；当<span style=\"color:red\">钇</span>的质量分数为2．67％时，析出相为α—Mg、Mg12YZn和Mg3Y2Zn3相；随着<span style=\"color:red\">钇</span>含量的增多，合金的抗拉强度、屈服强度和伸长率先增大后减小，当<span style=\"color:red\">钇</span>的质量分数为2．67％时，合金的性能最佳，抗拉强度和屈服强度分别为250．4，125．3MPa，伸长率为12．73%。","authors":[{"authorName":"宋奇慧","id":"b46cede9-456f-48ef-bc0f-ec2f68eba6f6","originalAuthorName":"宋奇慧"},{"authorName":"王新年","id":"f3fbf829-b350-4f2f-87df-a83ee3292d14","originalAuthorName":"王新年"},{"authorName":"朱兆军","id":"b6208716-8401-48f2-8caa-fdd7b0100b7e","originalAuthorName":"朱兆军"}],"doi":"","fpage":"21","id":"8f633d56-76ad-4c18-997b-5895b58e855f","issue":"7","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"e4972430-1893-404a-9299-785792d29127","keyword":"镁锌锆合金","originalKeyword":"镁锌锆合金"},{"id":"b7158d36-85e2-482d-bddb-2baa714fad66","keyword":"组织","originalKeyword":"组织"},{"id":"49a1aae0-8767-432f-a478-dc2b03a6644b","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"b1381fc9-f440-428a-94e8-ad8048a20b5a","keyword":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>","originalKeyword":"钇元素"}],"language":"zh","publisherId":"jxgccl201207007","title":"<span style=\"color:red\">钇</span>含量对铸态镁锌锆合金组织及力学性能的影响","volume":"36","year":"2012"},{"abstractinfo":"用井式电阻炉制备了不同<span style=\"color:red\">钇</span>含量的Mg-9Al-2.25Sr耐热镁合金,借助OM、SEM、EDS、XRD以及力学性能试验机等研究<span style=\"color:red\">钇</span>含量对合金显微组织和力学性能的影响.结果表明:<span style=\"color:red\">钇</span>可细化试验镁合金的组织,与铝结合生成弥散分布的颗粒状Al2Y高温相,有效抑制了β-Mg17Al12低温相的析出；在<span style=\"color:red\">钇</span>质量分数为0.35％时,合金的晶粒组织细小均匀,综合力学性能最优,其在室温和高温(200℃)下的抗拉强度、屈服强度分别为207.65,159.77MPa和192.52,134.83MPa.","authors":[{"authorName":"张金玲","id":"642450a4-f730-4c0d-bc59-e8c64ecb3699","originalAuthorName":"张金玲"},{"authorName":"刘璐","id":"d0b60e66-37e8-4534-975a-a98d60466153","originalAuthorName":"刘璐"},{"authorName":"王昕","id":"ed76b0d3-67c8-43d6-9c96-2c704fff9097","originalAuthorName":"王昕"},{"authorName":"范晋平","id":"53548554-831a-408c-bd24-285a6d37c8bd","originalAuthorName":"范晋平"},{"authorName":"王社斌","id":"55375f49-44f1-45dc-8cfa-fa9216b4df46","originalAuthorName":"王社斌"}],"doi":"","fpage":"5","id":"157cb63e-774b-4470-95be-58521afb563d","issue":"3","journal":{"abbrevTitle":"JXGCCL","coverImgSrc":"journal/img/cover/JXGCCL.jpg","id":"45","issnPpub":"1000-3738","publisherId":"JXGCCL","title":"机械工程材料"},"keywords":[{"id":"00a73f1d-aeca-4f6d-8c4c-82b95f0206d6","keyword":"耐热镁合金","originalKeyword":"耐热镁合金"},{"id":"4d7364ef-1eea-4bd5-9c91-8fd82c41396f","keyword":"<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>","originalKeyword":"钇元素"},{"id":"f9b9a966-1f7e-4d7a-9162-3acbb5e6ad1c","keyword":"显微组织","originalKeyword":"显微组织"},{"id":"a0027fe8-caa1-45d4-ac62-4f9a998fadeb","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"jxgccl201303002","title":"<span style=\"color:red\">钇</span>含量对Mg-9Al-2.25Sr耐热镁合金组织及力学性能的影响","volume":"37","year":"2013"},{"abstractinfo":"基于现有低碳钢焊条性能的特点,针对典型低碳钢焊条(E4303型焊条)抗裂性较差的问题,在新型低碳钢焊条药皮配方开发研制中采取药皮过渡微量的镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>.通过冲击韧性、拉伸、硬度、金相等试验研究镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>对低碳钢焊条熔敷金属组织和力学性能的影响,利用扫描电子显微镜对显微组织进行观察分析,用X射线荧光光谱仪进行光谱分析.结果表明:加入适量的镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>能够细化熔敷金属显微组织,提高熔敷金属的冲击韧性.当镧<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>加入量最佳(3.5%镧和0.6%<span style=\"color:red\">钇</span>)时,熔敷金属的冲击韧性提高了38.8%,延伸率提高了25%,抗拉强度提高了11.9%,屈服强度提高了10.9%,硬度却不下降.","authors":[{"authorName":"郭永环","id":"8dd11045-c831-4ba6-abf9-d2344255a291","originalAuthorName":"郭永环"},{"authorName":"范希营","id":"8c452b9b-a8e8-4b80-8c38-28ccc5c21b96","originalAuthorName":"范希营"},{"authorName":"王广丰","id":"5b3e056e-9c97-48fa-a68c-1e1cd5b90311","originalAuthorName":"王广丰"}],"doi":"","fpage":"272","id":"c65ce22b-bc69-4adc-a08c-3d5fb8d780bc","issue":"2","journal":{"abbrevTitle":"ZGXTXB","coverImgSrc":"journal/img/cover/ZGXTXB.jpg","id":"86","issnPpub":"1000-4343","publisherId":"ZGXTXB","title":"中国稀土学报"},"keywords":[{"id":"2fc6c0af-0ba7-4fc2-ace5-b905c6ed3a1f","keyword":"镧","originalKeyword":"镧"},{"id":"c7320eb3-8ff2-4f49-a618-e5f979dc9469","keyword":"<span style=\"color:red\">钇</span>","originalKeyword":"钇"},{"id":"c0952749-a03a-48c1-bb45-5f18c0ce68ea","keyword":"低碳钢焊条","originalKeyword":"低碳钢焊条"},{"id":"c43c4bda-f473-451b-9596-942c7161e98a","keyword":"熔敷金属","originalKeyword":"熔敷金属"},{"id":"d5e7c2da-2a92-434a-99a2-7cb0ab9d3d2d","keyword":"组织","originalKeyword":"组织"},{"id":"885fbfcf-5a8e-4806-89bf-665498b64133","keyword":"力学性能","originalKeyword":"力学性能"},{"id":"9cae8ffb-302c-40d2-b653-0e6542d3cac1","keyword":"稀土","originalKeyword":"稀土"}],"language":"zh","publisherId":"zgxtxb200902021","title":"镧、<span style=\"color:red\">钇</span><span style=\"color:red\">元素</span>对低碳钢焊条熔敷金属影响的研究","volume":"27","year":"2009"},{"abstractinfo":"采用机械合金化及热压烧结工艺制备了掺杂0.07%～1.35%(质量分数)稀土<span style=\"color:red\">元素</span><span style=\"color:red\">钇</span>的Laves相NbCrz合金,研究了<span style=\"color:red\">钇</span>含量对NbCrz合金在1 100℃氧化行为的影响,并探讨了其作用机制.结果表明:只有添加适量的<span style=\"color:red\">钇</span>(0.07%～0.14%)才能降低NbCr2合金的氧化速率,提高NbCr2合金的抗氧化性能;NbCr2合金高温抗氧化性能的提高,主要是由于稀土<span style=\"color:red\">元素</span><span style=\"color:red\">钇</span>增强了氧化膜与基体的结合性能.","authors":[{"authorName":"郑海忠","id":"53440c91-df06-402d-82b9-356840742ece","originalAuthorName":"郑海忠"},{"authorName":"鲁世强","id":"3df51e18-cd7d-4c8b-bc32-1cfd32a92deb","originalAuthorName":"鲁世强"},{"authorName":"闵嗣林","id":"96e499a1-a69f-4d4d-9c14-0c013b4a947e","originalAuthorName":"闵嗣林"},{"authorName":"崔霞","id":"0fd80c31-e103-4f4f-8838-35da386ff84a","originalAuthorName":"崔霞"}],"doi":"","fpage":"94","id":"f1a15093-1121-4dcf-865a-21b1e5cb22{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"","authors":[{"authorName":"王茹林","id":"1381a134-f7a1-4b61-8414-bf98e0a083e2","originalAuthorName":"王茹林"},{"authorName":"杨郁","id":"e9ba46d3-82a3-4e85-a404-d154624ebaec","originalAuthorName":"杨郁"},{"authorName":"双少敏","id":"7d0cb31d-a70d-4cd6-98bf-5996555c90c0","originalAuthorName":"双少敏"},{"authorName":"潘景浩","id":"49fa1a15-ed73-4d19-ad89-c950b3dfa9a1","originalAuthorName":"潘景浩"}],"doi":"10.3969/j.issn.1000-0518.2002.07.023","fpage":"702","id":"b6cee653-59d2-4fa5-8c23-e4a398a2bde5","issue":"7","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"8c95cc2c-bdac-4783-b481-34539a3c8e3e","keyword":"相溶解度","originalKeyword":"相溶解度"},{"id":"56adc052-7aa9-41f3-b01b-60cff3babdb1","keyword":"β-环糊精衍生物","originalKeyword":"β-环糊精衍生物"},{"id":"71975117-ed46-4620-b76d-ab87d71a3090","keyword":"<span style=\"color:red\">黄酮类药物</span>","originalKeyword":"黄酮类药物"},{"id":"83f4529b-f3cf-4644-8ead-e8b115f89386","keyword":"增溶作用","originalKeyword":"增溶作用"}],"language":"zh","publisherId":"yyhx200207023","title":"β-环糊精衍生物对<span style=\"color:red\">黄酮类药物</span>的增溶作用","volume":"19","year":"2002"},{"abstractinfo":"应用高速逆流色谱法分离制备了陈皮中3种<span style=\"color:red\">黄酮类</span>化合物.以石油醚-乙酸乙酯-甲醇-水(体积比为2∶4∶3∶3)为两相溶剂系统,在主机转速850 r/min、流动相流速1.7 mL/min、检测波长280 nm条件下进行分离制备,6 h 内从 4.0 g 陈皮粗提物中一步分离制备得到橙皮苷10.1 mg、桔皮素49.8 mg和 5-羟基-6,7,8,3′,4′-五甲氧基<span style=\"color:red\">黄酮</span>50.6 mg,纯度均达97.0%以上,各化合物结构经质谱和核磁共振氢谱、碳谱鉴定.利用该方法可以对陈皮中的<span style=\"color:red\">黄酮类</span>化合物进行快速的分离和纯化.","authors":[{"authorName":"孙印石","id":"8c497a37-6d80-4942-813f-31526e3307b4","originalAuthorName":"孙印石"},{"authorName":"刘政波","id":"dcc0e85f-1080-49cf-8bcd-b12055f5bbd6","originalAuthorName":"刘政波"},{"authorName":"王建华","id":"1bca4abe-b06b-40bb-8352-c0b1a2ab4ae8","originalAuthorName":"王建华"},{"authorName":"王迎","id":"1cb53741-6e81-4b47-a4a5-a12f92d9eb1e","originalAuthorName":"王迎"},{"authorName":"祝丽香","id":"8aa4f18a-294d-41b6-8ef4-0867eca63e80","originalAuthorName":"祝丽香"},{"authorName":"李来玲","id":"d2e26c88-e021-4269-864f-70ad96a13c04","originalAuthorName":"李来玲"}],"doi":"10.3321/j.issn:1000-8713.2009.02.024","fpage":"244","id":"8cb9b6c0-5222-4f1d-ac70-11021952f7ae","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"6beab011-d30f-4765-89be-d6f09444c7f2","keyword":"高速逆流色谱","originalKeyword":"高速逆流色谱"},{"id":"22fea808-f8fb-4e25-91db-5050e44f1606","keyword":"橙皮苷","originalKeyword":"橙皮苷"},{"id":"25df97db-6b1c-4158-a7f3-d0ce7832342c","keyword":"桔皮素","originalKeyword":"桔皮素"},{"id":"8fa40f89-caed-4048-b66c-b833e5423c16","keyword":"5-羟基-6,7,8,3′,4′-五甲氧基<span style=\"color:red\">黄酮</span>","originalKeyword":"5-羟基-6,7,8,3′,4′-五甲氧基黄酮"},{"id":"40116b78-5f2c-4d0b-85f9-e9fd5cb16a8e","keyword":"陈皮","originalKeyword":"陈皮"}],"language":"zh","publisherId":"sp200902024","title":"高速逆流色谱分离制备陈皮中的<span style=\"color:red\">黄酮类</span>化合物","volume":"27","year":"2009"},{"abstractinfo":"该文建立了大孔树脂-高速逆流色谱分离薇甘菊中<span style=\"color:red\">黄酮类</span>物质的方法.分离条件为:采用大孔树脂AB-8,洗脱液为50%(v/v)乙醇水溶液,高速逆流色谱溶剂体系为正丁醇-乙酸-水(4∶1∶5, v/v).从薇甘菊中分离到4种<span style=\"color:red\">黄酮类</span>物质:槲皮素-3-O-芸香糖苷(纯度90.2%)、山奈酚-3-O-芸香糖苷(纯度98.55%)、木犀草苷(纯度98.33%)和紫云英苷(纯度99.23%).建立的大孔树脂-高速逆流色谱方法简单、高效,可扩展应用于从其他植物中分离<span style=\"color:red\">黄酮类</span>物质.","authors":[{"authorName":"耿姗","id":"d09eb2c0-02e2-47ee-9040-ab3dbaa0b2f8","originalAuthorName":"耿姗"},{"authorName":"王娟强","id":"0bf9efe1-fc84-47bf-8be7-84ce4654197c","originalAuthorName":"王娟强"},{"authorName":"席兴军","id":"d2ea8460-4ff5-4e99-aa5f-2bff8493472d","originalAuthorName":"席兴军"},{"authorName":"初侨","id":"9596dcbf-3f82-4ae6-9b05-ab53ee952e8e","originalAuthorName":"初侨"},{"authorName":"董跟来","id":"88deb747-e8e1-42f2-87a2-07f5f54adae7","originalAuthorName":"董跟来"},{"authorName":"马晓萌","id":"22ccccb7-50da-441c-b81a-85eb955d32d8","originalAuthorName":"马晓萌"},{"authorName":"张惠文","id":"7c9ffe61-7803-4ee5-9f80-12b7ad491d2c","originalAuthorName":"张惠文"},{"authorName":"魏芸","id":"8625c4ae-0797-4bd5-b343-c7fe7007f1d7","originalAuthorName":"魏芸"}],"doi":"10.3724/SP.J.1123.2016.10022","fpage":"302","id":"671ee8c4-d79a-4d72-9d39-8d53c698073a","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"63f5b7e9-0e56-46cf-b5b3-0b1ac01484e4","keyword":"高速逆流色谱","originalKeyword":"高速逆流色谱"},{"id":"a40082f3-7c62-4fc6-8e4b-ac554e64e705","keyword":"大孔树脂","originalKeyword":"大孔树脂"},{"id":"032c486f-2e23-4408-9326-4de17c4d5d8e","keyword":"分离","originalKeyword":"分离"},{"id":"d7598223-7a02-4305-ac56-9867c1457531","keyword":"<span style=\"color:red\">黄酮类</span>物质","originalKeyword":"黄酮类物质"},{"id":"e9a69886-0f97-4d65-a768-c53d5019f3cc","keyword":"薇甘菊","originalKeyword":"薇甘菊"}],"language":"zh","publisherId":"sp201703015","title":"大孔树脂-高速逆流色谱分离纯化薇甘菊中的<span style=\"color:red\">黄酮类</span>化合物","volume":"35","year":"2017"},{"abstractinfo":"采用均匀实验设计和信息理论评价方法,建立了鱼腥草中<span style=\"color:red\">黄酮类</span>成分的高效液相色谱(HPLC)指纹图谱的分析方法.采用建立的方法和本研究室提出的指纹图谱评价软件,对同样种植条件下10个批次的鱼腥草指纹图谱进行了相似性评价,相似度均大于0.90;同时测定了芦丁、槲皮甙和槲皮素3个成分在10批鱼腥草药材中的含量分别为0.25% ～0.34% 、0.27% ～0.37% 、0.012% ～0.016% .另外对不同采收季节和不同部位的鱼腥草药材中的<span style=\"color:red\">黄酮类</span>成分进行了指纹图谱的测定、主成分分析以及成分含量测定,结果表明,不同季节、不同部位的鱼腥草中<span style=\"color:red\">黄酮类</span>化合物的指纹图谱及成分含量存在较大的差异,且药用部位的差异大于采收季节的差异.该方法为规范鱼腥草中<span style=\"color:red\">黄酮类</span>成分在制药和用药的实际应用提供了一些可靠的基础信息.","authors":[{"authorName":"卢红梅","id":"cc267da6-3268-4253-b133-c9082bc2ea8c","originalAuthorName":"卢红梅"},{"authorName":"彭丽华","id":"a67601bd-3c08-4128-882a-a4850b1dc37c","originalAuthorName":"彭丽华"},{"authorName":"郭方遒","id":"cbdfdc82-2acb-4d72-9a28-e5d3505a5860","originalAuthorName":"郭方遒"},{"authorName":"伍贤进","id":"b9b69813-24da-40b4-a3c9-0cfa539c6f11","originalAuthorName":"伍贤进"},{"authorName":"梁逸曾","id":"6bf13e06-b6eb-42e2-8943-f434ee7b19c1","originalAuthorName":"梁逸曾"}],"doi":"10.3724/SP.J.1123.2010.00965","fpage":"965","id":"3be50db4-caf0-49ca-a2bb-4c4b78b63078","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"bcc5b50a-d980-4983-b5ee-96874ffad0f7","keyword":"高效液相色谱","originalKeyword":"高效液相色谱"},{"id":"614279bc-5236-4b34-9945-881cb33669d9","keyword":"指纹图谱","originalKeyword":"指纹图谱"},{"id":"3cedce27-1151-4f1a-a65d-9376e1a2b49a","keyword":"<span style=\"color:red\">黄酮</span>","originalKeyword":"黄酮"},{"id":"49cd69dd-87fa-4a6d-a204-9b491ffa29ed","keyword":"鱼腥草","originalKeyword":"鱼腥草"}],"language":"zh","publisherId":"sp201010011","title":"鱼腥草中<span style=\"color:red\">黄酮类</span>成分的高效液相色谱指纹图谱分析","volume":"28","year":"2010"},{"abstractinfo":"应用高速逆流色谱法分离制备了乌药叶中的<span style=\"color:red\">黄酮类</span>成分.以正己烷-乙酸乙酯-正丁醇-冰醋酸-水(体积比为2:4:2:1.5:6)为两相溶剂系统,在主机转速800 r/min、流速2.0 mL/min、检测波长280 nm条件下进行分离制备.所得流分经高效液相色谱法检测,并经电喷雾电离质谱、核磁共振氢谱、碳谱鉴定化合物的结构.结果表明,从乌药叶总<span style=\"color:red\">黄酮</span>粗提物中分离得到了5个化合物,分别为槲皮素-3-O-β-D-葡萄糖苷(1)、槲皮素-5-O-β-D-葡萄糖苷(2)、槲皮素-3-O-β-D-呋喃阿拉伯糖苷(3)、槲皮素-3-O-吡喃鼠李糖苷(4)、山奈酚-7-O-α-L-吡喃鼠李糖苷(5),其中化合物1,2,3和5 为首次从该植物中分离得到.该法具有简便、快速的优点.","authors":[{"authorName":"刘云","id":"877392c6-2a4d-4cd4-bbfc-baa6fbb7af34","originalAuthorName":"刘云"},{"authorName":"侴桂新","id":"b8c45219-a23d-4dea-8687-e65daf41adea","originalAuthorName":"侴桂新"}],"doi":"10.3321/j.issn:1000-8713.2007.05.024","fpage":"735","id":"b362b839-90a4-4c50-bc36-4936283c9d15","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"28c542aa-0367-49bb-b749-a18ca25b596e","keyword":"高速逆流色谱","originalKeyword":"高速逆流色谱"},{"id":"9f0e7e0b-2840-4035-b0af-3f8c9e6d9576","keyword":"<span style=\"color:red\">黄酮类</span>成分","originalKeyword":"黄酮类成分"},{"id":"01b2bf7f-1709-4d7b-b181-6706c61c69a8","keyword":"乌药叶","originalKeyword":"乌药叶"}],"language":"zh","publisherId":"sp200705024","title":"高速逆流色谱法分离制备乌药叶中的<span style=\"color:red\">黄酮类</span>成分","volume":"25","year":"2007"},{"abstractinfo":"采用高效制备液相色谱法从荷叶(Nelumbo nucifera Gaertn)中分离制备荷叶<span style=\"color:red\">黄酮类</span>化合物.用60%乙醇回流提取荷叶,粗提液浓缩后经D-101柱及聚酰胺柱色谱分离,再在Symmetry PrepTM C18柱上分离,以水-乙腈为流动相进行梯度洗脱(流速为5.0 mL/min),得到了3种<span style=\"color:red\">黄酮类</span>化合物.经紫外光谱、红外光谱、核磁共振及质谱分析,确定该3种物质分别为金丝桃苷、异槲皮苷和紫云英苷.所制备的3种化合物的纯度都在97%以上,其中紫云英苷为首次从荷叶中分离得到.","authors":[{"authorName":"田娜","id":"5cb213b2-c421-4ec3-bab1-08386826685a","originalAuthorName":"田娜"},{"authorName":"刘仲华","id":"8a1853fe-01f3-4956-9aeb-0a8e6f735304","originalAuthorName":"刘仲华"},{"authorName":"黄建安","id":"3cc79ddd-bccf-44df-a97f-d5960d59e049","originalAuthorName":"黄建安"},{"authorName":"罗国安","id":"d13827bd-637d-4cb8-8f4a-2d2f8b7678c8","originalAuthorName":"罗国安"},{"authorName":"刘硕谦","id":"8ee98946-cfe8-4db3-ab1a-1e8c5a9151ae","originalAuthorName":"刘硕谦"},{"authorName":"刘新桃","id":"1f9ae6f9-8b8b-474a-8d8e-104058980159","originalAuthorName":"刘新桃"}],"doi":"10.3321/j.issn:1000-8713.2007.01.018","fpage":"88","id":"1deab512-f6dd-439a-bb78-4ea49b2ba3a8","issue":"1","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"7cd999bf-3cbe-423e-bf16-00ba329222f5","keyword":"制备型反相高效液相色谱法","originalKeyword":"制备型反相高效液相色谱法"},{"id":"c690074b-4b3a-448b-bfa7-35d146f7d5ad","keyword":"<span style=\"color:red\">黄酮类</span>化合物","originalKeyword":"黄酮类化合物"},{"id":"fa018ccd-27fc-4b74-bf03-59be61601133","keyword":"荷叶","originalKeyword":"荷叶"}],"language":"zh","publisherId":"sp200701018","title":"高效制备液相色谱法从荷叶中分离制备<span style=\"color:red\">黄酮类</span>化合物","volume":"25","year":"2007"},{"abstractinfo":"对蒙古黄芪中5种异<span style=\"color:red\">黄酮类</span>成分的含量进行了反相高效液相色谱法测定.色谱柱为Diamonsil C18柱,流动相为乙腈-水系统,梯度洗脱,检测波长230 nm,柱温35 ℃.毛蕊异<span style=\"color:red\">黄酮</span>-7-O-β-D-葡萄糖苷在20.12～201.2 mg/L、芒丙花素-7-O-β-D-葡萄糖苷在4.62～46.2 mg/L、9,10-二甲氧基紫檀烷-3-O-β-D-葡萄糖苷在4.86～48.6 mg/L、毛蕊异<span style=\"color:red\">黄酮</span>在9.24～92.4 mg/L、芒丙花素在6.92～69.2 mg/L时峰面积与浓度呈良好的线性关系,相关系数分别为0.999 2,0.999 7,0.999 7,0.999 5和0.999 5.5种成分的加样回收率均高于94%,相对标准偏差(RSD)小于3.2%(n=9).该法简便快速,重复性良好,结果准确可靠,可用于黄芪药材中5种主要异<span style=\"color:red\">黄酮类</span>成分的含量测定.","authors":[{"authorName":"王晓辉","id":"890ffe1e-de5a-4dc4-97ff-5e0a8ce090fa","originalAuthorName":"王晓辉"},{"authorName":"刘涛","id":"2abd2c8b-01fd-4191-9322-2d5027ce317c","originalAuthorName":"刘涛"},{"authorName":"李清","id":"a2e25111-a5e2-4abd-aa6b-83a640ba122a","originalAuthorName":"李清"},{"authorName":"陈晓辉","id":"f8e399ad-3edd-40d5-adfd-18abd8e59b77","originalAuthorName":"陈晓辉"},{"authorName":"毕开顺","id":"f20851c5-5f36-4470-a36a-196e022ceb7d","originalAuthorName":"毕开顺"}],"doi":"10.3321/j.issn:1000-8713.2006.05.014","fpage":"486","id":"ac3861b2-261d-4848-83be-d06e5604ad36","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5df2f20a-58cd-4e8a-8250-f304f50fd3f9","keyword":"反相高效液相色谱法","originalKeyword":"反相高效液相色谱法"},{"id":"f43f51c7-ef73-4579-998e-acdc35c17e43","keyword":"异<span style=\"color:red\">黄酮</span>","originalKeyword":"异黄酮"},{"id":"8b2bab5f-065c-4e04-bfeb-74bc3e91c25a","keyword":"黄芪","originalKeyword":"黄芪"}],"language":"zh","publisherId":"sp200605014","title":"高效液相色谱法同时测定黄芪中的五种异<span style=\"color:red\">黄酮类</span>成分","volume":"24","year":"2006"},{"abstractinfo":"应用高速逆流色谱法分离纯化了九里香中的4种<span style=\"color:red\">黄酮类</span>化合物.以石油醚-乙酸乙酯-甲醇-水(5:5:4.8:5,v/v/v/v)作为两相溶剂系统,上相为固定相,下相为流动相,以主机转速800 r/min、流速2.0 mL/min、单次进样量200 mg的条件成功地从4.0 g九里香粗提物中分离纯化出54.31 mg 5,7,3′,4′,5′-五甲氧基<span style=\"color:red\">黄酮</span>(重结晶后)、107.68 mg 5-羟基-6,7,3′,4′-四甲氧基<span style=\"color:red\">黄酮</span>、215.54 mg 5-羟基-6,7,8,3′,4′-五甲氧基<span style=\"color:red\">黄酮</span>、84.36 mg 5-羟基-6,7,8,3′,4′,5′-六甲氧基<span style=\"color:red\">黄酮</span>,纯度均在95%以上.各化合物的结构均由质谱和核磁共振氢谱、碳谱鉴定.其中化合物5-羟基-6,7,3′,4′-四甲氧基<span style=\"color:red\">黄酮</span>为首次从九里香中分离得到.","authors":[{"authorName":"彭爱一","id":"81f59124-50c7-4adc-9a01-29d59913d0e2","originalAuthorName":"彭爱一"},{"authorName":"曲学伟","id":"fac0ba8d-05a9-48cc-93ce-fcf46e9159d6","originalAuthorName":"曲学伟"},{"authorName":"李慧","id":"c2347734-4b1a-4e86-b63c-941366bbfe34","originalAuthorName":"李慧"},{"authorName":"高璐","id":"cae6d55e-3c3a-4de3-9a77-9023d7297f84","originalAuthorName":"高璐"},{"authorName":"于波","id":"6c3c26b4-b4b8-4b2d-9336-f4fd857d0db1","originalAuthorName":"于波"},{"authorName":"杨红","id":"406f1906-4c5d-4edb-bb76-812096db966d","originalAuthorName":"杨红"}],"doi":"10.3724/SP.J.1123.2010.00383","fpage":"383","id":"7887a2ff-5f7f-4307-ae63-f4c5f1df0ea1","issue":"4","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"4882b4d9-7827-400e-8783-0e39842b5fe5","keyword":"高速逆流色谱","originalKeyword":"高速逆流色谱"},{"id":"d053e007-9225-4daf-a6d5-7c51319a4750","keyword":"<span style=\"color:red\">黄酮类</span>化合物","originalKeyword":"黄酮类化合物"},{"id":"81d05f12-4ee4-45ec-8471-f8c4e7c45e7e","keyword":"九里香","originalKeyword":"九里香"},{"id":"6f552d07-4cb4-4a27-9495-0fd834195b3c","keyword":"中药","originalKeyword":"中药"}],"language":"zh","publisherId":"sp201004011","title":"高速逆流色谱分离纯化九里香中的<span style=\"color:red\">黄酮类</span>化合物","volume":"28","year":"2010"},{"abstractinfo":"建立了高效液相色谱同时测定枇杷叶中3种<span style=\"color:red\">黄酮类</span>成分的分析方法.该方法分析了不同产地枇杷叶中芦丁、槲皮素和山柰酚的含量差异.枇杷叶粉末用甲醇超声提取后,加盐酸回流,制备样品测试液.采用DiamonsilC18色谱柱(250 mm×4.6 mm,5μm),以0.4％ (v/v)磷酸水溶液-乙腈为流动相,梯度洗脱.分别对7个不同产地的枇杷叶样品中的芦丁、槲皮素和山柰酚进行测定.结果表明,芦丁、槲皮素、山柰酚在各自的质量浓度范围内线性关系良好(r＞0.99),加标回收率分别为96.33％、95.81％和95.80％,RSD分别为6.48％、0.90％和3.02％.该方法操作简单、分离度好、重复性高.不同产地枇杷叶中3种<span style=\"color:red\">黄酮类</span>成分的含量存在差异,其中芦丁的差异最大,而山柰酚的含量最稳定且在不同产地样品中均可检出,或可用作枇杷叶药材质量控制的标志成分.","authors":[{"authorName":"朱诗塔","id":"80cfe1a4-b561-449c-99f0-83bc2ff8d0a0","originalAuthorName":"朱诗塔"},{"authorName":"周巧玲","id":"14eb32b2-614c-48de-b17e-41572dc3cfc6","originalAuthorName":"周巧玲"},{"authorName":"金苹","id":"091a917f-0e92-4dc7-b6bc-64b8f697afc5","originalAuthorName":"金苹"},{"authorName":"肖瑶","id":"b1cee955-363b-45f3-9292-aff65ff914b3","originalAuthorName":"肖瑶"}],"doi":"10.3724/SP.J.1123.2016.07022","fpage":"1011","id":"7c551380-ad7d-4b5c-a9b1-bec686bf713d","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"05f3382d-1d96-4d3a-a5bb-2545af4f8119","keyword":"高效液相色谱","originalKeyword":"高效液相色谱"},{"id":"07bc4fd3-5c25-4878-9ce2-7739590ce390","keyword":"<span style=\"color:red\">黄酮类</span>","originalKeyword":"黄酮类"},{"id":"fb462d89-3809-401b-85e3-aa83a36056d3","keyword":"芦丁","originalKeyword":"芦丁"},{"id":"43b6db69-2d24-41c3-be6c-47ae753cee36","keyword":"槲皮素","originalKeyword":"槲皮素"},{"id":"f58dae82-c32d-45f4-b993-31aa17c681f4","keyword":"山柰酚","originalKeyword":"山柰酚"},{"id":"fa2b2491-4c4d-41d5-87fa-02e9f78aa1bc","keyword":"产地","originalKeyword":"产地"},{"id":"4bfad5c2-0d8a-4277-bc7f-4f44a766ac4e","keyword":"枇杷叶","originalKeyword":"枇杷叶"}],"language":"zh","publisherId":"sp201610016","title":"高效液相色谱法测定不同产地枇杷叶中的3种<span style=\"color:red\">黄酮类</span>成分","volume":"34","year":"2016"},{"abstractinfo":"采用高效毛细管电泳法分离测定了新疆不同地区、不同采集期、不同品种的桑叶中的<span style=\"color:red\">黄酮类</span>成分芦丁、槲皮素的含量.以含有体积分数为15%甲醇的10 mmol/L的磷酸二氢钠-20 mmol/L的硼砂溶液(pH 8.62)为电泳缓冲液,采用压力进样方式,在25 ℃,20 kV恒压下进行电泳分离,并在245 nm波长处检测.结果表明,桑叶中的两种目标组分在12 min内完全分离,且有良好的线性关系;芦丁和槲皮素的加样回收率分别为95.64%和99.36%,其RSD分别为2.25%和1.79%(n=6).方法简单、准确、快速.","authors":[{"authorName":"孙莲","id":"a694ee9b-35f2-4d49-8f9c-5bb305e30c74","originalAuthorName":"孙莲"},{"authorName":"孟磊","id":"77fe8840-3635-4334-a566-7f91ed9bd313","originalAuthorName":"孟磊"},{"authorName":"陈坚","id":"d513590c-5484-4f22-bfab-6360014a87bb","originalAuthorName":"陈坚"},{"authorName":"马季","id":"20e5ce65-22ea-4ea9-af55-b158749549db","originalAuthorName":"马季"},{"authorName":"胡瑞","id":"e98ee404-99b8-4639-92b8-9baad2c90bf4","originalAuthorName":"胡瑞"},{"authorName":"贾殿增","id":"a152ae7c-a1dd-45e4-a6bf-049e18989caf","originalAuthorName":"贾殿增"}],"doi":"10.3321/j.issn:1000-8713.2001.05.003","fpage":"395","id":"51063798-e33c-4735-bd15-0bf558c0f9fa","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"54c66cc6-412c-4b4e-b4a9-926323c9e8c2","keyword":"高效毛细管电泳","originalKeyword":"高效毛细管电泳"},{"id":"4d9d7ef5-f68c-49e9-9560-0ebb6275dcac","keyword":"芦丁","originalKeyword":"芦丁"},{"id":"81e36a2d-1437-4239-a162-297f92b5cc10","keyword":"槲皮素","originalKeyword":"槲皮素"},{"id":"0134f281-7d6e-4371-b2a5-f99363f34e20","keyword":"桑叶","originalKeyword":"桑叶"}],"language":"zh","publisherId":"sp200105003","title":"毛细管电泳法测定桑叶中的<span style=\"color:red\">黄酮类</span>成分芦丁和槲皮素","volume":"19","year":"2001"}],"totalpage":128,"totalrecord":1278}