{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用XRD、FESEM及色度测试等多种分析方法,研究了矿化剂种类、组合方式及添加量对(YAl_(1-x)Cr_xO_3)色料性能的影响.结果表明:适合于该色料的矿化剂有单一矿化剂CaF_2、二元复合矿化剂NaF+CaCO_3和三元矿化剂LiF+MgF_2+Na_2CO_3,促使晶形发育完善和呈色的综合效果为:CaF_2>NaF+CaCO_3>LiF+MgF_2+Na_2CO_3.矿化剂NaF+CaCO_3合成的色料主晶相为钇铝榴石(AlYO_3),次晶相为二钇铝榴石(Al_2Y_4O_9),残余相是Y_2O_3,另外两种矿化剂合成的色料则没有次晶相出现.NaF+CaCO_3的添加量在8%～12%(质量分数,下同)、CaF_2的添加量在13%～17%时,色料有较好的红度值.","authors":[{"authorName":"曹春娥","id":"65d2bb24-af7d-4f13-87e5-3f2025fa64a0","originalAuthorName":"曹春娥"},{"authorName":"洪琛","id":"a17ad151-f2f2-4cca-a685-3ca4057c3183","originalAuthorName":"洪琛"},{"authorName":"陈云霞","id":"8d3cfd31-6938-4a17-b4d3-0a80a6a0e37e","originalAuthorName":"陈云霞"},{"authorName":"余峰","id":"94fb73c5-953d-4a22-b503-584b16d3ae3d","originalAuthorName":"余峰"},{"authorName":"卢希龙","id":"ae83d30c-6c72-48c7-93ba-3b87619109fb","originalAuthorName":"卢希龙"},{"authorName":"沈华荣","id":"c284a1bd-0923-4e40-b835-75967799905a","originalAuthorName":"沈华荣"},{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"33f26236-d887-4dc1-9adb-0e3c9e03bbfc","originalAuthorName":"熊春华"},{"authorName":"郑乃章","id":"dc36b1a4-3a4a-4032-8071-2a4722c72232","originalAuthorName":"郑乃章"}],"doi":"","fpage":"118","id":"770d657e-25eb-407a-bcf3-a5e0b41885db","issue":"z2","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"b96fbf7d-3d4a-416d-8f31-9ad21dbb71b6","keyword":"陶瓷红色料","originalKeyword":"陶瓷红色料"},{"id":"bc1fa8f6-9bfd-4e16-879d-f5d332f99fc3","keyword":"钙钛矿型","originalKeyword":"钙钛矿型"},{"id":"2b5fee40-404c-4077-9502-f2c72a4e332c","keyword":"矿化剂","originalKeyword":"矿化剂"},{"id":"4e789797-c45f-4e80-8c0c-c65316f88a69","keyword":"性能","originalKeyword":"性能"}],"language":"zh","publisherId":"xyjsclygc2009z2032","title":"矿化剂对YAl_(1-x)Cr_xO_3陶瓷红色料性能的影响","volume":"38","year":"2009"},{"abstractinfo":"以工业硼酸、硼砂和氧化钙为原料,通过改变反应温度和原料配比,用水热法合成了系列硼钙化合物.根据化学分析和XRD分析数据确定了各种合成产物的化学组成、物相名称,用场发射扫描电镜(FE-SEM)对六种硼酸钙的显微形貌、颗粒大小进行了表征,发现它们的显微形貌、颗粒大小有很大的不同.CaO·3B2O3·5H2O呈条板状,厚度在100～300 nm之间;2CaO·5B2O3·5H2O呈大纳米薄片,厚度在50～100 am的居多;2CaO·3B2O3·H2O则是纳米细线,直径在100 nm左右;4CaO·5B2O3·7H2O呈小纳米薄片状,厚度在100 nm左右;2CaO·B2O3·H2O呈球粒状,大小在500 am～1μm;CaO·B2O3呈粗针状,粗、细端直径在150～300 nm之间.","authors":[{"authorName":"曹春娥","id":"665edb0e-960d-48f3-807f-08e4e3a20a55","originalAuthorName":"曹春娥"},{"authorName":"曹惠峰","id":"d884024b-ef4a-46db-a71e-ae240e16bd67","originalAuthorName":"曹惠峰"},{"authorName":"卢希龙","id":"a5fbd3f9-c653-41ae-8218-b6e26cc0d929","originalAuthorName":"卢希龙"},{"authorName":"余峰","id":"48920bcf-7478-47b4-8ec7-e503cae362e4","originalAuthorName":"余峰"},{"authorName":"郎莹","id":"208db0c0-666a-4775-9f2e-d1a2a743efe2","originalAuthorName":"郎莹"},{"authorName":"沈华荣","id":"0e3ced0c-7d10-481e-9b2b-9dd836185c1a","originalAuthorName":"沈华荣"},{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"5988c0c5-9daa-4263-b150-bf0f09ddc224","originalAuthorName":"熊春华"},{"authorName":"郑乃章","id":"1ec9d972-473e-43e3-ade2-962e64d0904c","originalAuthorName":"郑乃章"}],"doi":"","fpage":"1228","id":"96835c96-4a39-4f65-871a-9d2715cdcbc8","issue":"5","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"2dba3d05-d69c-483a-aaa6-6836b52e98bc","keyword":"硼酸钙","originalKeyword":"硼酸钙"},{"id":"0291cbf7-0388-4d94-9f3d-e6153e8055bc","keyword":"水热合成","originalKeyword":"水热合成"},{"id":"0882f961-d4c4-4233-be4d-5c99a513e79a","keyword":"FE-SEM分析","originalKeyword":"FE-SEM分析"}],"language":"zh","publisherId":"rgjtxb98200805040","title":"水热法合成硼酸钙的场发射扫描电镜分析","volume":"37","year":"2008"},{"abstractinfo":"采用XRD、FESEM及EDS等多种分析方法,研究了Cr2O3含量对铬钇铝红(YAl1-xCrxO3)色料物相组成和显微结构的影响,探讨了Cr3+取代部分Al3+离子后,色料主晶相(YAlO3)、次晶相(Al2Y4O9)、残余相的变化及显微结构的不同.结果表明:随着Cr2O3含量的增加,合成色料颗粒由圆粒状长成典型的钙钛矿型立方形晶体和由于畸变形成的类四方形晶体;立方和类四方形颗粒为主晶相,圆粒状颗粒中Y2O3含量比主晶相中的高;由于立方型向正方型的晶格畸变,晶胞参数有所改变;当x为0.05～0.13时,色料有最好的红度值,此时主晶相晶形完整,大小均匀,发育良好.","authors":[{"authorName":"曹春娥","id":"23c23d80-02c1-4cc1-82bd-a83b870f01d5","originalAuthorName":"曹春娥"},{"authorName":"洪琛","id":"e61832a9-eb22-4274-894d-3466e08df9ff","originalAuthorName":"洪琛"},{"authorName":"郎莹","id":"a18d6717-e947-4dec-b38c-c9959832ca13","originalAuthorName":"郎莹"},{"authorName":"宋福生","id":"d771fa97-61b5-4f2d-9886-7420d68f44fb","originalAuthorName":"宋福生"},{"authorName":"余峰","id":"c990d265-41d6-4f63-b7cb-b8461ca67a42","originalAuthorName":"余峰"},{"authorName":"沈华荣","id":"fdf1e793-a857-4d9f-b53f-e6643b8f0f11","originalAuthorName":"沈华荣"},{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"c94e6241-3dca-4438-83b3-8282f2807c12","originalAuthorName":"熊春华"},{"authorName":"卢希龙","id":"39fa65d1-0f1a-4cc9-be9a-ca62a7560c80","originalAuthorName":"卢希龙"}],"doi":"","fpage":"699","id":"f360ac8a-bb56-409a-a20f-3fae6953f456","issue":"3","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"efa30420-4b1e-4930-9797-778ccf0b78e6","keyword":"陶瓷色料","originalKeyword":"陶瓷色料"},{"id":"c3e55665-9641-4b6e-ae63-74f4f0183bbb","keyword":"钙钛矿型","originalKeyword":"钙钛矿型"},{"id":"7f23d134-bd81-485c-920e-79bf28a5e9d4","keyword":"Cr2O3含量","originalKeyword":"Cr2O3含量"},{"id":"fd4947a3-65f0-4d74-be78-b9403fc77b06","keyword":"物相组成","originalKeyword":"物相组成"},{"id":"af4f01d6-78bf-454c-8ce5-0ce2635304b4","keyword":"显微结构","originalKeyword":"显微结构"}],"language":"zh","publisherId":"rgjtxb98200803040","title":"Cr2O3含量对YAl1-xCrxO3红色料物相组成与显微结构的影响","volume":"37","year":"2008"},{"abstractinfo":"以CaO-B2O3-H2O系统为研究体系,用硼酸和氧化钙做起始原料,采用湿化学合成法制备了四水六硼酸钙粉料.研究了起始原料浓度、系统的pH值对四水六硼酸钙合成的影响,用DTA、XRD、TEM、FESEM、化学分析等研究了合成工艺过程,并对合成产物进行了定性定量分析.结果表明:氧化钙与硼酸的摩尔比在(0.09～0.15)∶1范围,硼酸与水的摩尔比在(0.3～0.45)∶1范围,以氨水为添加剂调节pH值为7,反应温度为90～100 ℃时将生成四水六硼酸钙.TEM观察发现多数晶体呈片状、条状,有些呈准六方晶片聚集状,颗粒大小多数在0.2～0.3 μm之间;用FESEM观察可看到这些晶片自发排列成球形的晶蔟.","authors":[{"authorName":"曹春娥","id":"e3b8022f-fe72-47cc-984d-eecd9064111e","originalAuthorName":"曹春娥"},{"authorName":"卢希龙","id":"35615619-8de8-4402-9840-b010ed31a6e7","originalAuthorName":"卢希龙"},{"authorName":"余峰","id":"670472a8-0f5f-4492-ad15-fed816ddc274","originalAuthorName":"余峰"},{"authorName":"沈华荣","id":"e01a803a-f254-47de-a401-cf0cacbe013b","originalAuthorName":"沈华荣"},{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"72461a79-fb0f-48ce-a97d-ac7a408404a8","originalAuthorName":"熊春华"},{"authorName":"郑严艳","id":"6a33d06e-4158-4884-bfe5-3464dd470901","originalAuthorName":"郑严艳"},{"authorName":"曹惠峰","id":"e00867f6-de6e-45a5-85e7-355ad5114e55","originalAuthorName":"曹惠峰"},{"authorName":"郑乃章","id":"162de488-704d-43bf-9d9e-fc576a05463d","originalAuthorName":"郑乃章"}],"doi":"","fpage":"118","id":"ff244637-968d-4262-9f52-10297719eaf7","issue":"z1","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"b4d92153-2a9f-43c2-8f8d-04c758b676cf","keyword":"硼酸钙","originalKeyword":"硼酸钙"},{"id":"44a20b5b-c6e0-4445-8d65-83536a62516a","keyword":"湿化学合成","originalKeyword":"湿化学合成"},{"id":"09a29ab9-c9bc-4640-b31b-3d6be29a2b74","keyword":"pH值","originalKeyword":"pH值"},{"id":"6dd42749-6022-4e55-968a-78ba91d0afce","keyword":"添加剂","originalKeyword":"添加剂"},{"id":"38924edd-5c7c-44ba-96cb-050c0f3699bd","keyword":"表征","originalKeyword":"表征"}],"language":"zh","publisherId":"xyjsclygc2007z1035","title":"硼酸、氧化钙合成四水六硼酸钙的工艺参数研究与性能表征","volume":"36","year":"2007"},{"abstractinfo":"","authors":[{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"eceed52e-d3c1-4910-973a-0bd021037a4b","originalAuthorName":"熊春华"},{"authorName":"沈秋仙","id":"d44b8eec-d72c-4954-8235-11ed398d29fe","originalAuthorName":"沈秋仙"}],"doi":"","fpage":"492","id":"065b6864-a976-485d-85c1-3091a3496212","issue":"5","journal":{"abbrevTitle":"XTXBYWB","coverImgSrc":"journal/img/cover/XTXBEN.jpg","id":"66","issnPpub":"1002-0721","publisherId":"XTXBYWB","title":"稀土学报(英文版)"},"keywords":[{"id":"463c678c-c6a6-464b-9861-71421fe46d9c","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"zgxtxb-e200205037","title":"Adsorption of Er(Ⅲ) and Its Mechanism on Diglycolamidic Acid Resin","volume":"20","year":"2002"},{"abstractinfo":"研究了铈(Ⅲ)在氨基磷酸树脂上的吸附行为。试验结果在pH5.0时，静态饱和吸附容量为197mg/g干树脂；用2mol.L-1HCl洗脱，洗脱率为98.1%；表观速率常数k298=2.71×10-5s-1；等温吸附服从Freundlich经验式；吸附反应中的△Ho=50.0kJ.mol-1，△So=286J.mol-1.K-1，△Go=-35.1kJ.mol-1。树脂功能基与Ce3+的配比为2∶1；并用红外光谱探讨了树脂与铈的成键。","authors":[{"authorName":"王永江","id":"9fc8b321-1b14-456d-b23a-7055f41bc069","originalAuthorName":"王永江"},{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"3fda055f-3502-425b-ad46-22632443fe41","originalAuthorName":"熊春华"},{"authorName":"舒增年","id":"69bed795-d073-4237-8ba0-f691476fd0df","originalAuthorName":"舒增年"},{"authorName":"王惠君","id":"7211a2af-e4c7-45cb-83b9-3a5e1efc90b4","originalAuthorName":"王惠君"}],"doi":"10.3969/j.issn.1004-0277.2001.02.006","fpage":"17","id":"20dba158-486e-45b7-8b25-a70ae0bfbab6","issue":"2","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"0d022ab3-e497-4c62-9cec-6850ab0431ac","keyword":"氨基膦酸树脂","originalKeyword":"氨基膦酸树脂"},{"id":"173ffd05-8d16-480d-ae9c-aacc89264759","keyword":"铈","originalKeyword":"铈"},{"id":"4bd806bd-eea4-4455-94e4-d78551b5a039","keyword":"吸附","originalKeyword":"吸附"}],"language":"zh","publisherId":"xitu200102006","title":"氨基膦酸树脂吸附铈的研究","volume":"22","year":"2001"},{"abstractinfo":"","authors":[{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"7f2402c8-0b00-40b6-8e44-5c66c0b8ee40","originalAuthorName":"熊春华"},{"authorName":"沈秋仙","id":"33bc49bf-6a3f-4ff2-a077-5f45e8cffea3","originalAuthorName":"沈秋仙"}],"doi":"","fpage":"492","id":"3d1d1883-f1b8-4f6b-ba98-c4f1e40e3a8d","issue":"5","journal":{"abbrevTitle":"XTXBYWB","coverImgSrc":"journal/img/cover/XTXBEN.jpg","id":"66","issnPpub":"1002-0721","publisherId":"XTXBYWB","title":"稀土学报(英文版)"},"keywords":[{"id":"f4ba7dae-b5ba-43f9-af7b-36f7cb05eebe","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"zgxtxb-e200205037","title":"Adsorption of Er(Ⅲ) and Its Mechanism on Diglycolamidic Acid Resin","volume":"20","year":"2002"},{"abstractinfo":"以CoCl2·6H2O和AlCl3为原料,NaOH为沉淀剂,采用水热法合成尖品石型纳米钻蓝色料.主要研究合成温度和保温时间对CoAl2O4色料主晶相、呈色的影响,采用XRD,TEM,FTIR,TG-DTA分光光度计等分析测试技术对合成产物进行表征.结果表明,在245℃/20h能制备出纯度较高的纳米CoAl2O4,其晶型完整、粒度均匀,粒径多为70nm左右,此时的色饱和度和色度值也达最佳.","authors":[{"authorName":"胡琪","id":"cd48a612-afbf-4cfb-b8ce-56a0150362ca","originalAuthorName":"胡琪"},{"authorName":"曹春娥","id":"ccdedc60-59d8-4ed5-a1bd-cbd75d768c29","originalAuthorName":"曹春娥"},{"authorName":"陈云霞","id":"0da2b189-4a8d-45be-9bdd-206b90e06bf9","originalAuthorName":"陈云霞"},{"authorName":"沈华荣","id":"699ddd72-0037-45bd-8fbe-a5a054f26a57","originalAuthorName":"沈华荣"},{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"256e0016-632e-4b10-b4af-c66608617d02","originalAuthorName":"熊春华"}],"doi":"10.3969/j.issn.1001-4381.2010.z2.101","fpage":"366","id":"5308a528-52c2-4992-a968-ee97946194c0","issue":"z2","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"e761f996-c73c-4cb4-9667-f430a9476dd7","keyword":"CoAl2O4色料","originalKeyword":"CoAl2O4色料"},{"id":"cbc92885-fadb-4291-9aa2-e62a865066b2","keyword":"纳米","originalKeyword":"纳米"},{"id":"64498e17-7023-481c-9405-a0e91de660f3","keyword":"水热法","originalKeyword":"水热法"},{"id":"d506ddfc-0c95-4407-b4ea-99e69a22b47d","keyword":"合成温度","originalKeyword":"合成温度"},{"id":"1f2956fa-aada-47f4-95f2-b362e79998b0","keyword":"保温时间","originalKeyword":"保温时间"}],"language":"zh","publisherId":"clgc2010z2101","title":"水热合成温度与保温时间对纳米COAl2O4色料性能的影响","volume":"","year":"2010"},{"abstractinfo":"","authors":[{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"fee4a33a-06d1-466b-8e8d-1d725b644b31","originalAuthorName":"熊春华"},{"authorName":"沈秋仙","id":"0d892064-e9d9-485c-8fe3-b861a1d3b5e0","originalAuthorName":"沈秋仙"}],"doi":"","fpage":"492","id":"79965f21-4369-4e08-bf9b-5d76d1ddb561","issue":"5","journal":{"abbrevTitle":"XTXBYWB","coverImgSrc":"journal/img/cover/XTXBEN.jpg","id":"66","issnPpub":"1002-0721","publisherId":"XTXBYWB","title":"稀土学报(英文版)"},"keywords":[{"id":"fddbf02d-b8e1-470e-b98d-1e1269b8730f","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"zgxtxb-e200205037","title":"Adsorption of Er(Ⅲ) and Its Mechanism on Diglycolamidic Acid Resin","volume":"20","year":"2002"},{"abstractinfo":"以海藻酸钠为原料,氯化钙/甘油/酒精溶液为凝固浴,采用冷冻干燥方法制备了海藻酸钙海绵,通过红外光谱和扫描电镜对其结构进行了表征,并对其物理和力学性能、孔隙率、透气率、吸液量和保液量进行评价和测定。结果表明,海藻酸钙海绵的弹性和柔韧性好,具有均匀、连通的孔隙结构,孔径大小为100μm～500μm,孔隙率为84.37%,透气率为44.75%,拉伸强度为0.21 MPa,初始模量为7.72 N/mm,对伤口渗出液的吸液量和保液量为30.48 g/g和5.13 g/g,各项性能均优于或接近海藻酸钙无纺布医用敷料。","authors":[{"authorName":"张传杰","id":"9d40905c-d1c2-46ff-bf51-af228cba7779","originalAuthorName":"张传杰"},{"authorName":"徐琪","id":"5166b88f-325b-4826-9ed5-da8762c95262","originalAuthorName":"徐琪"},{"authorName":"<span style=\"color:red\">熊</span><span style=\"color:red\">春华</span>","id":"5656ca53-8367-4047-a884-29ace215032e","originalAuthorName":"熊春华"},{"authorName":"冉建华","id":"96d1b974-c3c1-4bf4-ac76-ef4deab7894e","originalAuthorName":"冉建华"},{"authorName":"刘云","id":"e03407dd-e067-4697-860f-6518053d16ec","originalAuthorName":"刘云"},{"authorName":"朱平","id":"7a2bc12d-5ec5-4db7-8b8b-f92ee63cbf80","originalAuthorName":"朱平"}],"doi":"","fpage":"24","id":"7f95cf13-ba4a-4490-b267-f6e295c8a0df","issue":"9","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"49a56549-08df-48d6-afab-205fc7e2e2c8","keyword":"海藻酸钙","originalKeyword":"海藻酸钙"},{"id":"8316e876-d71a-4d69-b831-676b59795768","keyword":"海绵","originalKeyword":"海绵"},{"id":"653a62a7-0a67-464d-b71c-e7edfb3db02e","keyword":"医用敷料","originalKeyword":"医用敷料"},{"id":"a3d41d3e-f712-4c81-ba5a-2efde5c9bed9","keyword":"吸湿性","originalKeyword":"吸湿性"},{"id":"17820302-8f0f-4ecb-abb6-80a461cbd38c","keyword":"力学性能","originalKeyword":"力学性能"}],"language":"zh","publisherId":"gfzclkxygc201209007","title":"海藻酸钙海绵的结构与性能","volume":"28","year":"2012"}],"totalpage":6,"totalrecord":54}