{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"采用冷等离子体对碳纤维缝编织物进行表面处理,并采用XRD对处理前后的碳纤维表面结构进行了分析,研究了冷等离子体处理对浸润性以及碳纤维缝编织物/环氧复合材料的层间剪切强度的影响.实验结果表明,冷等离子体处理提高了碳纤维表面活性、浸润性,从而改善了碳纤维缝编织物/环氧复合材料的界面粘结性能,进而改善了复合材料的界面性能.","authors":[{"authorName":"秦伟","id":"9ba28d4a-5122-46bf-b1a7-e10122533426","originalAuthorName":"秦伟"},{"authorName":"张志谦","id":"da18d2e6-bff3-489a-9b52-90a3aae2bf53","originalAuthorName":"张志谦"},{"authorName":"黄玉东","id":"26b4fdeb-3401-4703-a1aa-14ea0431d108","originalAuthorName":"黄玉东"},{"authorName":"叶杨","id":"6ce75506-a4de-4abc-b0d4-e11390e2b232","originalAuthorName":"叶杨"},{"authorName":"<span style=\"color:red\">刘</span><span style=\"color:red\">爱</span><span style=\"color:red\">学</span>","id":"08405984-8876-41ba-8779-67cf41411263","originalAuthorName":"刘爱学"},{"authorName":"李海晨","id":"09aa2c32-48f7-45cb-9ae9-fcb0022ccd26","originalAuthorName":"李海晨"},{"authorName":"王彪","id":"eb1d07f2-b712-43a8-bf93-4db068ed2325","originalAuthorName":"王彪"}],"doi":"10.3969/j.issn.1005-5053.2001.04.009","fpage":"38","id":"af6adfe3-0c4b-4d1d-9247-ceb00b37ca92","issue":"4","journal":{"abbrevTitle":"HKCLXB","coverImgSrc":"journal/img/cover/HKCLXB.jpg","id":"41","issnPpub":"1005-5053","publisherId":"HKCLXB","title":"航空材料学报"},"keywords":[{"id":"7e2fd005-5d22-42b0-81fd-d4bdf718914e","keyword":"冷等离子体技术","originalKeyword":"冷等离子体技术"},{"id":"fa528d5d-48aa-4aef-b73a-dd085612660c","keyword":"碳纤维缝编织物","originalKeyword":"碳纤维缝编织物"},{"id":"b90072ab-ed36-489c-b8e9-744508bda806","keyword":"环氧复合材料","originalKeyword":"环氧复合材料"},{"id":"bfb660b3-9751-4d89-b2fb-3a549d4b3e83","keyword":"表面处理","originalKeyword":"表面处理"}],"language":"zh","publisherId":"hkclxb200104009","title":"冷等离子体处理对碳纤维缝编织物/环氧复合材料界面性能的影响","volume":"21","year":"2001"},{"abstractinfo":"为了改善浇铸聚酰胺6(MC-PA 6)的冲击韧性,制备了聚酰胺6-聚氨酯(PA 6-PU)嵌段共聚物.采用示差扫描量热分析(DSC)、动态力学性能分析(DMTA)以及静态力学性能测试研究了PU柔性组分对PA 6-PU嵌段共聚物结构和性能的影响.结果表明,当PU柔性组分含量为15%~20%(质量分数,下同)时,共聚物中出现了2个熔融峰,表明晶粒尺寸分布较宽;DMTA确定PA 6-Pu嵌段共聚物只有1个玻璃化温度(α松弛峰),说明共聚物为单相体系.PA 6-PU嵌段共聚物的力学性能数据表明,随PU组分含量的增加,共聚物的拉伸强度下降,但50℃和25℃时的冲击强度大幅度提高.","authors":[{"authorName":"邓鑫","id":"14e8a517-08ab-4e9f-b598-5d29a88ce5f1","originalAuthorName":"邓鑫"},{"authorName":"<span style=\"color:red\">刘</span><span style=\"color:red\">爱</span><span style=\"color:red\">学</span>","id":"a2ef4f46-f2a5-463a-89cc-f975624e8d5a","originalAuthorName":"刘爱学"},{"authorName":"王进","id":"e706b179-c3b9-40fc-8cbc-c6d91353c1b2","originalAuthorName":"王进"},{"authorName":"杨军","id":"362d0c97-775e-4b73-9b53-77d3e426a347","originalAuthorName":"杨军"},{"authorName":"李笃信","id":"1f0ac87e-a38f-41b4-8c87-5671d4914261","originalAuthorName":"李笃信"}],"doi":"","fpage":"14","id":"ec24bb8d-7cfb-40dd-8da4-c402360c11c8","issue":"6","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"bf9dac66-1b80-4b0e-84f0-0a2824864c9d","keyword":"聚酰胺6","originalKeyword":"聚酰胺6"},{"id":"195e4dea-77cf-4609-a851-d6d3746e4fdb","keyword":"聚氨酯","originalKeyword":"聚氨酯"},{"id":"e4df7509-6156-4a3b-8f27-506b2dc4f8be","keyword":"嵌段共聚物","originalKeyword":"嵌段共聚物"},{"id":"c07832df-34d1-4435-9e66-10b164de8473","keyword":"单体浇铸","originalKeyword":"单体浇铸"},{"id":"4b9ca74c-4500-4eba-8e9d-02384b6f092d","keyword":"增韧","originalKeyword":"增韧"}],"language":"zh","publisherId":"cldb201006005","title":"聚酰胺6-聚氨酯嵌段共聚物的制备及其性能研究","volume":"24","year":"2010"},{"abstractinfo":"通过自制的酚醛-纳米蒙脱土(PF-MMT)和γ-氨丙基三乙氧基硅烷-纳米埃洛石(KH550-HNTs)以不同质量配比复配改性PA6,研究了不同复配比例对PA6结晶性能、热稳定性、吸水性和力学性能的影响.结果表明:PF-MMT复配KH550-HNTs改性PA6提高了体系的热稳定性和抗吸水性,Tg变化不大,但结晶度下降.纳米PF-MMT复配KH550-HNTs/PA6复合材料的刚性得到提高,韧性有所下降,尤其是弯曲强度得到较大提高.","authors":[{"authorName":"赖登旺","id":"326148e2-69d8-45fa-a961-0979609eac44","originalAuthorName":"赖登旺"},{"authorName":"李笃信","id":"557c956d-2385-46b3-b7aa-06ea614ba2ea","originalAuthorName":"李笃信"},{"authorName":"杨军","id":"22cd3b7d-0b7f-4047-9941-7672fc136941","originalAuthorName":"杨军"},{"authorName":"<span style=\"color:red\">刘</span><span style=\"color:red\">爱</span><span style=\"color:red\">学</span>","id":"c22666e3-bec3-494b-8af0-aaa0646e20fb","originalAuthorName":"刘爱学"},{"authorName":"胡天辉","id":"8faa6933-812a-4f16-a09b-bf308f8ff3b7","originalAuthorName":"胡天辉"}],"doi":"","fpage":"22","id":"bcfb8a58-a64c-48c4-b733-0567cba7377e","issue":"4","journal":{"abbrevTitle":"FHCLXB","coverImgSrc":"journal/img/cover/FHCLXB.jpg","id":"26","issnPpub":"1000-3851","publisherId":"FHCLXB","title":"复合材料学报"},"keywords":[{"id":"bc410fa6-e9e5-485b-991d-3380fd69bb54","keyword":"蒙脱土","originalKeyword":"蒙脱土"},{"id":"3c6bab7b-53ba-4f5d-b96f-58ac2b923e36","keyword":"埃洛石","originalKeyword":"埃洛石"},{"id":"dc0c45aa-aede-498f-87ff-c20054671823","keyword":"尼龙6","originalKeyword":"尼龙6"},{"id":"0cd917d6-e046-4c4f-9e2d-fd19c6fd63af","keyword":"复配改性","originalKeyword":"复配改性"}],"language":"zh","publisherId":"fhclxb201304004","title":"酚醛-蒙脱土和KH550-埃洛石复配改性尼龙6的制备及性能","volume":"30","year":"2013"},{"abstractinfo":"以南京化学工业园的土壤为研究对象，分析土壤中重金属 Cr （Ⅵ）和 Pb 对赤子<span style=\"color:red\">爱</span>胜蚓（ Eisenia fetida）生长及繁殖的影响．结果表明，与对照组比较，暴露28 d时，较低浓度的Cr（Ⅵ）（4—8 mg·kg－1）和Pb （1000—1500 mg·kg－1）能促进赤子<span style=\"color:red\">爱</span>胜蚓的生长发育，而较高浓度的 Cr （Ⅵ）（32—64 mg·kg－1）和 Pb （3000 mg·kg－1）则显著抑制赤子<span style=\"color:red\">爱</span>胜蚓的生长发育；赤子<span style=\"color:red\">爱</span>胜蚓的产茧量随着Cr（Ⅵ）和Pb浓度的升高被显著抑制，其中，Cr（Ⅵ）抑制赤子<span style=\"color:red\">爱</span>胜蚓产茧量的EC50（半数有效浓度）、NOEC（无观察效应浓度）和LOEC（最低观察效应浓度）分别为22．86（20．56—25．42）、8、16 mg·kg－1．Pb抑制赤子<span style=\"color:red\">爱</span>胜蚓产茧量的EC50、NOEC和LOEC分别为2280．34（2200．90—2362．65）、1500、2000 mg·kg－1；与人工土壤中Cr（Ⅵ）和Pb对赤子<span style=\"color:red\">爱</span>胜蚓产茧量的28 d?EC50有显著性差异．","authors":[{"authorName":"王婉华","id":"56c0256b-8e9d-4416-8d00-2edbe16d5059","originalAuthorName":"王婉华"},{"authorName":"陈丽红","id":"82c06f44-bbd1-47d7-85ac-e87161293dd9","originalAuthorName":"陈丽红"},{"authorName":"<span style=\"color:red\">刘</span>征涛","id":"34013e0e-300a-47a1-9070-633565d7f135","originalAuthorName":"刘征涛"},{"authorName":"王晓南","id":"9861afea-5b8b-4eab-b0f2-a88f572fde40","originalAuthorName":"王晓南"},{"authorName":"张聪","id":"e3e42c92-bd94-4515-a584-20f19a33f6a7","originalAuthorName":"张聪"}],"doi":"10.7524/j.issn.0254-6108.2015.10.2015042102","fpage":"1839","id":"eb7346f9-7a48-4866-8f84-f151fae42a9a","issue":"10","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学   "},"keywords":[{"id":"22c25278-6ff3-4289-b46c-6d39e0877541","keyword":"Cr(Ⅵ)","originalKeyword":"Cr(Ⅵ)"},{"id":"8e5f019a-d464-4d25-9be2-62079ccad618","keyword":"Pb","originalKeyword":"Pb"},{"id":"b2ec3ebf-4267-4f92-9cdd-8b75ddd0d149","keyword":"南京土壤","originalKeyword":"南京土壤"},{"id":"01cbdd03-6b43-436d-a903-aa16fb01de6a","keyword":"人工土壤","originalKeyword":"人工土壤"},{"id":"7d8797cd-ca53-4118-8f3f-8ab316810eac","keyword":"赤子<span style=\"color:red\">爱</span>胜蚓","originalKeyword":"赤子爱胜蚓"},{"id":"145126d8-eb5f-4534-a3db-377047f31d87","keyword":"生长","originalKeyword":"生长"},{"id":"644ae44e-0c0d-470a-9a2d-90e245c9dc5f","keyword":"繁殖","originalKeyword":"繁殖"}],"language":"zh","publisherId":"hjhx201510011","title":"重金属铬（Ⅵ）和铅对南京土壤中赤子<span style=\"color:red\">爱</span>胜蚓生长及繁殖的影响?","volume":"","year":"2015"},{"abstractinfo":"<span style=\"color:red\">刘</span>文中,关于贝氏体形成机制,包括形核过程的文献很少被引述。作者（<span style=\"color:red\">刘</span>等）的主要论点为贝氏体铁素体以无扩散、非切变机制在奥氏体内贫碳区形核,并未引述形成贫碳区的必要条件。本文作者强调,在钢及铜合金中,不可能由Spinodal分解和位错偏聚形成贫溶质区。<span style=\"color:red\">刘</span>等的理念未得到先进理论观点和精细实验结果的支持。在<span style=\"color:red\">刘</span>文中,据此对临界核心大小和形核能的计算并无显著意义,期望青年学者对贝氏体相变机制作进一步研究。","authors":[{"authorName":"徐祖耀","id":"f5bc6b26-ec4d-45e7-a1da-067daa9d3115","originalAuthorName":"徐祖耀"}],"doi":"","fpage":"158","id":"66a9e9e8-09a0-408c-8c33-bc00aeff35c0","issue":"2","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"5224cfe0-dd6d-4ccc-aac3-2bed80f388a5","keyword":"贝氏体形核","originalKeyword":"贝氏体形核"},{"id":"cae16aae-8a2b-43f5-9886-1ca5759c5972","keyword":"扩散机制","originalKeyword":"扩散机制"},{"id":"36bc9f8f-ee13-4c27-8020-c2c5b0dfca8f","keyword":"切变机制","originalKeyword":"切变机制"},{"id":"a3bb808d-ba7a-4c9a-90ff-d5e59a6a0f1a","keyword":"贫碳区","originalKeyword":"贫碳区"}],"language":"zh","publisherId":"jsrclxb201202033","title":"评<span style=\"color:red\">刘</span>宗昌等《贝氏体铁素体的形核》一文","volume":"33","year":"2012"},{"abstractinfo":"利用质子激发X射线荧光分析(PIXE)测试分析汝官瓷、张公巷窑青瓷和<span style=\"color:red\">刘</span>家门窑青瓷样品的主要化学组成,用多元统计判别分析方法对数据进行分析,以确定它们的分类和起源关系.结果表明:汝官瓷、张公巷窑青瓷和<span style=\"color:red\">刘</span>家门窑青瓷釉基本能很好的区分；但是胎区分得不是很理想,张公巷窑青瓷的胎可以和汝官瓷、<span style=\"color:red\">刘</span>家门窑青瓷胎很好的区分,汝官瓷胎和<span style=\"color:red\">刘</span>家门窑青瓷胎有个别样品不能分开.","authors":[{"authorName":"蔡敏敏","id":"bf1f4660-208a-4999-ac81-266bf48c5bcb","originalAuthorName":"蔡敏敏"},{"authorName":"李国霞","id":"f8d3a4dc-7472-4dd6-9382-9f4430feef58","originalAuthorName":"李国霞"},{"authorName":"赵维娟","id":"9572b140-eca3-4192-af6e-ab9fdb21502b","originalAuthorName":"赵维娟"},{"authorName":"李融武","id":"e2d1fb82-016c-4ae3-9ee6-0cabbe60a2a0","originalAuthorName":"李融武"},{"authorName":"赵文军","id":"ea875a05-c1f7-4a8f-b405-2005de7db87c","originalAuthorName":"赵文军"},{"authorName":"承焕生","id":"9ff5fa85-a1fb-4cd2-bdc3-3bd240fd6894","originalAuthorName":"承焕生"},{"authorName":"郭敏","id":"d4074d21-787e-429b-8123-a13fcf5ce433","originalAuthorName":"郭敏"}],"doi":"","fpage":"1363","id":"f1ea8842-b3fe-42a2-9557-aa4c186cac5a","issue":"6","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"d281b6ff-a4b5-41d8-ad69-47236e801de5","keyword":"汝官瓷","originalKeyword":"汝官瓷"},{"id":"adf8b648-9625-4b38-96ff-ec6174d0c5d4","keyword":"张公巷窑青瓷","originalKeyword":"张公巷窑青瓷"},{"id":"3a61e23c-a3f8-43e6-84fc-1b7cd4edef5b","keyword":"<span style=\"color:red\">刘</span>家门窑青瓷","originalKeyword":"刘家门窑青瓷"},{"id":"494e2983-99cd-4c53-a919-4bfad5b7c54a","keyword":"判别分析","originalKeyword":"判别分析"}],"language":"zh","publisherId":"gsytb201206005","title":"汝官瓷、张公巷窑青瓷和<span style=\"color:red\">刘</span>家门窑青瓷的判别分析研究","volume":"31","year":"2012"},{"abstractinfo":"建立了尿样中可卡因(COC)及其代谢物<span style=\"color:red\">爱</span>冈宁甲基酯(EME)的气相色谱检测方法. 采用液液萃取法提取尿样中可卡因和<span style=\"color:red\">爱</span>冈宁甲基酯,考察了萃取剂种类和用量、试样pH值以及萃取时间等因素对提取效果的影响. 结果表明,尿样中COC和EME的最佳液液萃取条件是:以V(氯仿)∶ V(异丙醇)=9∶ 1为提取溶剂,调节样品溶液pH=9.5,在40 ℃水浴振荡提取6 min. COC和EME日内精密度分别为1.73%和1.44%,日间精密度分别为2.57%和2.89%,最低检出限(LOD)为0.040 mg/L. 此法无需衍生化、快速、准确、灵敏度高,可同时检测尿样中COC和EME的含量.","authors":[{"authorName":"叶能胜","id":"a1cfee26-8466-4f01-9a91-4a5af72095f5","originalAuthorName":"叶能胜"},{"authorName":"王小波","id":"5e52dc4a-e5be-4e94-aed2-3810c3a32c78","originalAuthorName":"王小波"},{"authorName":"王继芬","id":"6cb547e8-6cd1-4bbb-849b-7246eaf98a54","originalAuthorName":"王继芬"},{"authorName":"谷<span style=\"color:red\">学</span>新","id":"81f0e322-86e9-4166-8d7b-6acdd07d52b6","originalAuthorName":"谷学新"}],"doi":"10.3724/SP.J.1095.2010.90847","fpage":"1221","id":"c63a4620-6100-4e3b-9839-faad838245ed","issue":"10","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"9f4e5e75-e840-4cc4-ace4-dbc1892e9542","keyword":"液液萃取","originalKeyword":"液液萃取"},{"id":"1c73371e-cc10-4c9e-abb4-cd9437acc471","keyword":"气相色谱","originalKeyword":"气相色谱"},{"id":"8510917b-03f0-4b3b-977f-b20e51a508fc","keyword":"可卡因","originalKeyword":"可卡因"},{"id":"ae9ebe34-214a-47b4-9143-bb34b90db16b","keyword":"<span style=\"color:red\">爱</span>冈宁甲基酯","originalKeyword":"爱冈宁甲基酯"},{"id":"08018102-8d9a-4015-a5d5-59195827b038","keyword":"尿液","originalKeyword":"尿液"}],"language":"zh","publisherId":"yyhx201010020","title":"气相色谱法测定尿液中可卡因及其代谢物<span style=\"color:red\">爱</span>冈宁甲基酯","volume":"27","year":"2010"},{"abstractinfo":"本文采用质子激发X射线荧光分析(PIXE)技术测试了34个汝官瓷样品、30个蓝色系列钧官瓷样品(不含红釉系列)和17个<span style=\"color:red\">刘</span>家门窑青瓷样品的主量化学组成含量,根据这些样品的主量化学组成含量数据,应用多元统计分析方法进行分析.结果表明:汝官瓷、钧官瓷和<span style=\"color:red\">刘</span>家门窑青瓷的釉样品能够较好的区分开;但是3种瓷胎并不能很好的分开.","authors":[{"authorName":"肖朋飞","id":"6c5bc42f-0f99-48b4-b412-749a9ae0e046","originalAuthorName":"肖朋飞"},{"authorName":"赵红梅","id":"27edfee9-f617-4a36-af10-1a11a2aec85c","originalAuthorName":"赵红梅"},{"authorName":"李融武","id":"019184bd-8770-4aad-9618-4e2e6642f646","originalAuthorName":"李融武"},{"authorName":"赵文军","id":"6c10bb80-2026-4274-9965-bf564b102cc6","originalAuthorName":"赵文军"},{"authorName":"李国霞","id":"6f63b95a-67cb-4f68-b4b5-7c0b6f8f38e7","originalAuthorName":"李国霞"},{"authorName":"赵维娟","id":"ee11e4bc-a40c-4de3-90c4-e81dd16a55e3","originalAuthorName":"赵维娟"},{"authorName":"承焕生","id":"528f9874-c9c9-4258-bc3c-5a0d9ea8b362","originalAuthorName":"承焕生"}],"doi":"","fpage":"312","id":"3b352bdd-7627-42ad-a3b3-45e88dc561eb","issue":"2","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"080b7cee-826f-4a82-af62-9feed6531e66","keyword":"汝官瓷","originalKeyword":"汝官瓷"},{"id":"684a6128-65b6-45ce-be61-e74720b4c844","keyword":"钧官瓷","originalKeyword":"钧官瓷"},{"id":"14ccb09f-07d1-4f4b-bb41-c0ad3eea1fa0","keyword":"<span style=\"color:red\">刘</span>家门窑青瓷","originalKeyword":"刘家门窑青瓷"},{"id":"4b254520-d0a1-406e-a9ef-92267cd23fb0","keyword":"PIXE","originalKeyword":"PIXE"},{"id":"12b26595-24a4-4ea9-b303-ae046a74c72d","keyword":"因子分析","originalKeyword":"因子分析"}],"language":"zh","publisherId":"gsytb201102013","title":"汝官瓷、钧官瓷和<span style=\"color:red\">刘</span>家门窑青瓷的多元统计分析","volume":"30","year":"2011"},{"abstractinfo":"阐述了基于传统<span style=\"color:red\">爱</span>泼斯坦(Epstein)方圈法的电工钢片磁性能测量技术的新进展,主要涉及排除方圈角部双搭接结构区域被测试样磁性能不均匀性影响的双Epstein方圈法,以及考虑了方圈不同部位总比损耗不同的磁路长度加权处理法.通过分析以Epstein方圈法为基础的直流偏磁工况磁测量技术发展现状和存在的问题,对方圈法在直流偏磁性能测量技术方面的应用及发展进行了展望.","authors":[{"authorName":"高洁","id":"23baea47-68ba-4a4e-9f95-462991450b43","originalAuthorName":"高洁"},{"authorName":"杨富尧","id":"92fee45a-cbba-402d-b475-b388a411e753","originalAuthorName":"杨富尧"},{"authorName":"马光","id":"d8b26b05-ca15-4689-ba88-4a53ffa55d15","originalAuthorName":"马光"},{"authorName":"程灵","id":"ef23c806-873e-4912-901d-445f6143f4b8","originalAuthorName":"程灵"},{"authorName":"陈新","id":"fc0b60a5-ed1e-4470-96d3-bb497cfc7283","originalAuthorName":"陈新"},{"authorName":"孔晓峰","id":"af6539a3-c58c-45e6-a14f-3503cc19848c","originalAuthorName":"孔晓峰"}],"doi":"10.11896/j.issn.1005-023X.2016.03.023","fpage":"121","id":"394944fd-bed5-4785-96e3-905298f32219","issue":"3","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"8c18e62e-264d-4c24-9873-a921dab0772d","keyword":"磁特性测量","originalKeyword":"磁特性测量"},{"id":"fe91a88a-dddc-4a5b-ad81-b2ac7ad2272a","keyword":"电工钢片","originalKeyword":"电工钢片"},{"id":"33f00d97-24fb-4a75-8dba-10a16fc56131","keyword":"直流偏磁","originalKeyword":"直流偏磁"},{"id":"f1663b11-37d3-416b-b220-4e96368a258a","keyword":"<span style=\"color:red\">爱</span>泼斯坦方圈","originalKeyword":"爱泼斯坦方圈"}],"language":"zh","publisherId":"cldb201603023","title":"<span style=\"color:red\">爱</span>泼斯坦方圈法及其在直流偏磁性能测量方面的应用研究现状及展望","volume":"30","year":"2016"},{"abstractinfo":"建立了血液中可卡因(cocaine, COC)及其代谢物<span style=\"color:red\">爱</span>冈宁甲基酯(ecgonine methyl ester, EME)的气相色谱-质谱(CG-MS)和气相色谱-氢火焰离子化检测(GC-FID)方法.该方法采用微波萃取提取血液中的COC和EME,优化并确定了最佳提取条件:以氯仿-异丙醇(体积比为9:1)混合溶液为提取溶剂,用0.05 mol/L Na2CO3-NaHCO3缓冲溶液调节样品溶液的pH至10.0,在40 ℃下微波萃取6 min;采用GC-MS对萃取液中的COC和EME进行定性,采用GC-FID进行定量检测.COC和EME的平均回收率分别为79.91%～99.85%,相对标准偏差(RSD)均小于3.10% ,检出限(S/N=3)分别为60 mg/L 和40 mg/L.该方法无需衍生化,快速、准确、灵敏,可同时检测血液中的COC和EME.","authors":[{"authorName":"王小波","id":"c7134ec0-4975-4889-aa09-e24c4e4799a2","originalAuthorName":"王小波"},{"authorName":"叶能胜","id":"a192c2af-e54e-4011-8a52-126bad552387","originalAuthorName":"叶能胜"},{"authorName":"王继芬","id":"fb0b4413-07ec-40dc-819d-b385fc172b0a","originalAuthorName":"王继芬"},{"authorName":"谷<span style=\"color:red\">学</span>新","id":"3740f94b-5d58-44cf-a5ae-a61e13f238ca","originalAuthorName":"谷学新"}],"doi":"10.3724/SP.J.1123.2010.00673","fpage":"673","id":"e4df9454-c510-47d1-960f-189b2444307a","issue":"7","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"1c34095c-9594-4845-9849-7ca819fe63ea","keyword":"微波萃取","originalKeyword":"微波萃取"},{"id":"f5f7eae1-de8f-4c60-a5fe-e9349c1d9592","keyword":"气相色谱-质谱","originalKeyword":"气相色谱-质谱"},{"id":"1611deb5-c650-409a-80ca-740fd677a8cf","keyword":"气相色谱-火焰离子化检测","originalKeyword":"气相色谱-火焰离子化检测"},{"id":"b7ac94d3-8918-423f-a89f-0e909e06b9e2","keyword":"可卡因","originalKeyword":"可卡因"},{"id":"c4a28d9d-8c84-4733-a0dd-ad55cec120fa","keyword":"<span style=\"color:red\">爱</span>冈宁甲基酯","originalKeyword":"爱冈宁甲基酯"},{"id":"26dbe844-3f71-462c-bda0-30592c82b0b5","keyword":"血液","originalKeyword":"血液"}],"language":"zh","publisherId":"sp201007008","title":"微波萃取-气相色谱法测定血液中的可卡因及其代谢物<span style=\"color:red\">爱</span>冈宁甲基酯","volume":"28","year":"2010"}],"totalpage":291,"totalrecord":2909}