H. Ying1)
,
X. D. Sun1)
,
Q. B. Yang1)
,
J. B. Li2)
,
Y. M. Wang2)
,
Z. Zhang3) and J. You3)1) School of Materials and Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China2) Departm ent of Materials
,
School of Mechanical Engineering
,
Shenyang University
,
Shenyang110044
,
China3) Liaoning Analyzing and Testing Research Center
,
Shenyang 110015
,
China
金属学报(英文版)
Starting from cheap inorganic salts , ultrafine P L Z T po w ders were synthesized by a co pre cipitation m ethod . The results show that the precursor precipitate obtained by the co precipita tion method transfor ms co m pletely to P L Z T phase by calcining at 420 ℃ for 4 hours , about300 ℃low er than the nor m al transform ation te m perature of P L Z T obtained by m ixed oxidemethod . The effect of residual N H4 N O3 in the precursor precipitate on transfor m ation te m perature of the P L Z Tpow der w as investigated . The residual N H4 N O3 in the precursor po w der can reduce further the P L Z Ttransfor m ation tem perature to about 300 ℃, but a sm alla mount of Zr O2 and Pb Ti O3 re m ained . By a proper control of the synthesizing route , a P L Z T po w der with a pri m ary particle size of 10 n m and an agglom eration size of 0 3 μm hasbeen produced .
关键词:
P L Z T
,
null
,
null
F. Zhang1)
,
X. D. Sun1)
,
J. You2)
,
Z. Zhang2)
,
L. X. Ding3)and Y. M. Wang3)1) School of Materials and Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China2) Liaoning Analyzing and Testing Research Center
,
Shenyang 110015
,
China3) Department of Materials
,
School of Mechanical Engineering
,
Shenyang University
,
Shenyang 110044
,
China
金属学报(英文版)
Synthesis of a m m oniu m alu min u m carbonate hydroxide ( A A C H) w as investigated usinga m m oniu m alu min u m sulfate and a m moniu m hydro carbonate as the starting m aterials . Itw as found that A A C Hcan be synthesized by adding a m m oniu m alu m inu m sulfate solution torapidly stirred a m moniu m hydro - carbonate solution at a tem perature of 30 ℃. A A C Hcantransfor m to α Al2 O3 co m pletely by calcining at 1100 ℃ for 1 hour , and the obtained po w ders , with a particle size of 100 n m , can be sintered to 98 99 % relative density at 1500 ℃for 2 hours .
关键词:
a m moniu m alu m inu m carbonate hydroxide
,
null
,
null
,
null
Y. Q. Jia1)
,
J. G. Li1)
,
Y. M. Wang2)
,
L. X. Ding2)
,
X. M . Qin1) and X. D. Sun1)1) School of Materials and Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China2) Department of Materials
,
School of Mechanical Engineering
,
Shenyang University
,
Shenyang 110044
,
China
金属学报(英文版)
Using yttriu m nitrate as the m other salt , synthesis of ultrafine yttria po w der through w et che mical route w as investigated . Choice of precipitant has dra m atic effects on co m position ,particle size distribution and particle m orphology of the precipitates . When a m m onia solutionw as used as the precipitant , the precursor precipitate w as m ainly Y2( O H) 5 14( N O3) 0 86· H2 O with co m paratively large particle size , broad size distribution and co m plex particleshapes . When sodiu m hydroxide solution w as used , roughly spherical α Y( O H)3·3 H2 Opre cipitate w ith sm all particle size and narro w size distribution w as obtained . The transfor m a tion sequence of dry α Y( O H)3 ·3 H2 O gel during calcination w as determ ined to be α Y( O H) 3·3 H2 O→ Y O O H→ Y2 O3 . After calcining at 600 ℃ for 1 hour , both Y2( O H) 5 14( N O3) 0 86· H2 O and α Y( O H) 3·3 H2 O transfor m to well crystallized Y2 O3 pow ders ,w ith particle sizes of 50 ～3000 n m and 20 n m , respectively .
关键词:
KEYW ORDS yttria
,
null
,
null
,
null
H.W.Liu 1)
,
H.Ding 2) and J.Z.Cui 2) 1) School of Mechanical Engineering
,
Shenyang University
,
Shenyang 110044
,
China 2) School of Materials & Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China
金属学报(英文版)
Porthole dies are important tools in extrusion process to produce hollow sections and the life of the dies counts for the cost of products. In this work, the finite element method was adopted to analyze a particular porthole die to produce hollow rectangle sections which are widely used in construction. The upper die was mainly studied. Because it is symmetrical, a quarter of the die was analyzed. The upper die was divided into 2199 elements with 3018 nodes. Elements were produced by four steps and the geometric shape of the die could be well simulated. The boundary condition was given according to the shape of the welding chamber and an empirical average extrusion stress was adopted, which was 210N/mm 2. Three-dimensional equivalent stresses were received. The original porthole die studied had obvious stress concentration and the stress distribution was very inhomogeneous, which would heavily affect the die life. A new design was proposed in which the portholes were rearranged and their shape and dimension were changed. According to the finite element analysis, the stress distribution of the improved die was quite homogeneous and the stress concentration was lessened.
关键词:
section extrusion
,
null
,
null
H.W.Liu 1)
,
H.Ding 2) and J.Z.Cui 2) 1) School of Mechanical Engineering
,
Shenyang University
,
Shenyang 110044
,
China 2) School of Materials & Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China
金属学报(英文版)
The samples obtained by Finite Element Method (FEM) simulation for section extrusion process have been trained on BP Neural Networks. The mapping relationsbetween die's geometrical parameters and energetic parameters, such as stress and strain generated in the die are established. The extrusion process model and its expert system are also determined. The excellent expansibility this system possesses provides a new prospect for the future development of expert system for section extrusion dies.
关键词:
BP neural networks
,
null
,
null
,
null
X.W.Yin
,
L.F.Cheng
,
L.T.Zhang
,
W.C.Zhou and Y.D.Xu State Key Laboratory of Solidification Processing
,
Northwestern Polytechnical University
,
Xi′an 710072
,
China
金属学报(英文版)
Strong, tough, and almost fully dense C fiber reinforced celsian matrix composites have been fabricated by impregnation of the fiber tows with the matrix slurry, winding on a drum, drying, stacking the prepreg tapes in the desired orientation, and hot pressing. The monoclinic celsian phase in the matrix was produced in situ, during hot pressing, from amphosous BAS. The unidirectional composites having ≈20 vol% of fibers exhibited graceful failure with extensive fiber pullout in three point bend tests at room temperature. Values of ultimate flexural strength and fracture toughness were 379MPa and 8 3MPa·m 1/2 , respectively.
关键词:
barium aluminosilicate
,
null
,
null
,
null
,
null
Q. C. Le and J. Z. Cui School of Materials & Metallurgy
,
Northeastern University
,
Shenyang 110006
,
China
金属学报(英文版)
The 08 Al steel sheets were hot dip ped into Zn - Mn bath with 0 1 % Mn and 0 2 % Mn at600 ～420 ℃ bath tem perature , and then w ere treated in different w ays . The after - treat ments include cooling in the air at room tem perature directly , holding at the upper part of thehot dip galvanizing furnace for 60 s an d then holding at 510 ±10 ℃for 90 s . The results in dicated that blue , yellow , and purple , w hose coloration varied with the co m position an d thetem perature of bath and the w ays of after - treat ment . Finally , the mechanism of coloredzinc coating w as discussed .
关键词:
coloring hot dip galvanization
,
null
,
null
