Qing LIN
,
Lianzeng YAO
,
Guowei JIANG
,
Chuangui JIN
,
Weifeng LIU
,
Weili CAI
,
Zhen YAO
材料科学技术（英文）
Aligned silicon dioxide nanotubes with diameter of 60~70 nm were synthesized inside the nanoholes of an anodic Al membrane (AAM) template by pressure impregnating the AAM pores with the SiO¬2 sol. The SiO¬2 nanotubes with different wall thickness were produced by repeating the process. Using the second-order template of porous AAM with silicon dioxide nanotubes, it was fabricated the nanostructure of Fe nanowires encapsulated by SiO¬2 nanotubes by electrochemical deposition. Scanning electron microscope (SEM) and transmission electron microscope (TEM) observations show that the nanotubes and nanocables are compact, continuous and uniform. Selected area electron diffraction (SAED) pattern shows the Fe nanowire is a single crystal. The magnetic properties of these samples were checked by a vibrating sample magnetometer (VSM). The coercivities of the samples are greatly improved compared to the corresponding bulk materials.
关键词:
Template
,
null
,
null
,
null
Mingzai WU
,
Lianzeng YAO
,
Weili CAI
,
Guowei JIANG
,
Xiaoguang LI
,
Zhen YAO
材料科学技术（英文）
Ordered ZnO nanowire arrays embedded in anodic aluminum oxide (AAO) membranes were fabricated by electrochemical deposition of Zn(NO3)2+H3BO3 solution in a boiling bath. Scanning electron microscope (SEM) and transmission electron microscope (TEM) observation results show that the polycrystalline ZnO nanowires with diameters around 100 nm were uniformly assembled into the ordered nanochannels of the AAO. The results of the investigation into photoluminescence (PL) and electronic paramagnetic resonance (EPR) measurements reveal that the interfaces between the ZnO nanowires and the pore walls of the AAO create a lot of oxygen vacancies, which are responsible for the green light emission (peaking around 512 nm) and the huge enhancement of the PL emission.
关键词:
Nanowires
,
null
,
null
