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Characterization of Nanocrystalline Intermetallic Compound NiAl Synthesized by Condensation

Yong QIN , Xiaoying QIN and Lide ZHANG (Institute of Solid State Physics , Chinese Academy of Sciences , Hefei 230031 , China)(To whom correspondence should be addressed)

材料科学技术(英文)

Nanocrystalline intermetallic compound NiAl was Synthesized by evaporating NiAl master alloy in inert-gas followed by in situ compaction, and its structure was studied by means of X-ray diffractometry and transmission electron microscope. Experimental results reveal that the assynthesized nanocrystalline sample has a mean grain size of less than 10 nm and it is dominantly composed of the cubic structure phase NiAl. However, nanocrystalline Ni3Al as a trace phase mixed in NiAl phase, was also detected by transmission electron microscope observation.

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