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IN-SITU ELECTRON MICROSCOPY STUDY ON PRECIPITATION OF ZIRCONIUM HYDRIDES INDUCED BY STRESS AND STRAIN IN ZIRCALOY-2

ZHOU Bangxin ZHENG Sikui WANG Shunxin Southwest Centre for Nuclear Reactor Engineering Research and Design , Chengdu , China [Originally published in ACTA METALL SIN(CHINESE EDN)25(3)1989 pp A190—A195 , Southwest Centre for Nuclear Reactor Engineering Research and Design , Chengdu , China

金属学报(英文版)

The precipitation process of zirconium hydrides induced by stress and strain was investigated by means of electron microscopy in-situ.The precipitating hydrides induced by stress were found to be γ phase with orientation relationship of (110)_γ‖(110)_(αZr),(001)_γ‖ (0001)_(αZr) between γ-hydrides and surrounding matrix.The growth rate of γ-hydrides which was much faster along [110] direction brought them in taper shape.After fracture of y-hydrides,a new one will precipitate at the tip of cracks.This is the essential process of hydrogen-induced delayed cracking in Zircaloy.The precipitating hydrides induced by strain were found to be δ phase with both orientation relationships of(111)_δ‖(0001)_(αZr),(110)_δ‖ (110)_(αZr) or (010)_δ‖(0001)_(αZr),(001)_δ‖(110)_(αZr)between δ-hydride and surrounding matrix.The δ-hydrides become much finer as the strain rate increased.

关键词: Zircaloy-2 , null , null , null

Zr-2合金中应力及应变诱发氢化锆析出过程的电子显微镜原位研究

周邦新 , 郑斯奎 , 汪顺新

金属学报

用电子显微镜原位研究了Zr-2合金中的氢化锆在应力及应变作用下的析出过程。应力诱发析出的氢化锆为γ相,与基体间存在(110)_γ//(1120)_(αZr),(001)_γ//(0001)_(αZr)的取向关系。γ氢化锆沿它的[110]生长最快,形成尖劈状。当沿氢化锆开裂后,在裂纹端部又将析出氢化锆。应变诱发析出的氢化锆为δ相,与基体间存在(111)_δ//(0001)_(αZr),(110)_δ//(1120)_(αZr);或(010)_δ//(0001)_(αZr),(001)_δ//(1120)_(αZr)的取向关系。形变速率越高,δ氢化锆越细小。

关键词: Zr-2合金 , Precipitation of hydrides , hydrogen-induced delayed cracking

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