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Fe超微粒子的组织结构研究

王淑荷 , 蔡瑜玲 , 安刚 , 闻立时 , 庄育智

金属学报

本文采用X射线衍射、高分辨电镜和X射线光电子能谱仪对气相蒸发法所制备的Fe超微粒子的形态、组成、晶体结构和表面状态进行了研究。结果表明Fe超微粒子呈球形、直径大约20um,主要由心部的α-Fe和表面约4um厚的Fe_3O_4氧化物膜层所组成。并给出了超微粒子的高分辨点阵图象。

关键词: 超微粒子 , microstructure , high-resolution lattice image

MICROSTRUCTURAL STUDIES OF ULTRAFINE IRON PARTICLES

WANG Shuhe CAI Yuling AN Gang WEN Lishi ZHUANG Yuzhi Institute of Metal Research , Academia Sinica , Shenyang , China WANG Shuhe , Associate Professor , Institute of Metal Research , Academia Sinica , Shenyang 110015 , China

金属学报(英文版)

The constitution,structure and surface state of the ultrafine iron particles prepared by gas evaporation technique have been investigated by means of X-ray analysis,high-reasolution electron microscopy(HREM)and electron spectroscopy for chemical analysis(ESCA).The results showed that the fine particles are spherical ones of~20 nm in diameter with α-Fe cores and covered by Fe_3O_4 fine crystalline layers of~4 nm thickness.

关键词: ultrafine particle , null , null

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