{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"P84共聚聚酰亚胺能溶于常见的非质子溶剂进行湿法纺丝。良溶剂可以制得性能稳定的纺丝浆液,这对得到结构相对密实的聚酰亚胺纤维很重要。本文从聚合物和溶剂溶度参数的计算,P84共聚聚酰亚胺在不同溶剂中的特性黏度测试以及P84共聚聚酰亚胺/溶剂/水三元体系的相图三方面出发,比较分析了较适合P84共聚聚酰亚胺湿法纺丝的溶剂。结果表明,P84的溶度参数为10.35,与N-甲基吡咯烷酮(NMP)和N,N′-二甲基乙酰胺(DMAc)的溶度参数(分别为11.23和11.14)较接近;P84-NMP,P84-DMAc和P84-DMF的特性黏度分别是0.807,0.657和0.615;结合相图得到NMP、DMAc以及N,N′-二甲基甲酰胺(DMF)比较适合P84湿法纺丝,其中NMP最佳。","authors":[{"authorName":"向红兵","id":"8a9a4a81-f490-4ac9-a46b-1b831e656035","originalAuthorName":"向红兵"},{"authorName":"黄忠","id":"6e0061ac-9454-4982-9bfb-5b2bda60f281","originalAuthorName":"黄忠"},{"authorName":"诸静","id":"81001453-b750-4e00-9bb9-2efff241a79a","originalAuthorName":"诸静"},{"authorName":"陈蕾","id":"618679a3-dc99-4364-9d90-40d03c1ead05","originalAuthorName":"陈蕾"},{"authorName":"于俊荣","id":"2d720821-0c4b-46e6-9907-b149ba0a41fe","originalAuthorName":"于俊荣"},{"authorName":"胡祖明","id":"ba96953d-5b6f-4a89-ab07-ca81bcfd5bde","originalAuthorName":"胡祖明"}],"doi":"","fpage":"117","id":"ff0ef2b3-acd8-46fa-aa3f-75b30ae122e1","issue":"10","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"3fc98ded-89cb-4104-a1bd-ccfb469c9acf","keyword":"P84共聚聚酰亚胺","originalKeyword":"P84共聚聚酰亚胺"},{"id":"47b4d033-1b14-4335-985e-e06fc1019a51","keyword":"湿法纺丝","originalKeyword":"湿法纺丝"},{"id":"63e981e9-1a9b-48db-b837-4b381829a6cb","keyword":"特性黏度","originalKeyword":"特性黏度"},{"id":"b140078a-5a2c-49a4-ae00-4de34d127dea","keyword":"溶度参数","originalKeyword":"溶度参数"},{"id":"90377f67-6805-4576-a3c2-720550952aa5","keyword":"三元相图","originalKeyword":"三元相图"}],"language":"zh","publisherId":"gfzclkxygc201110037","title":"P84共聚聚酰亚胺湿法纺丝溶剂的选择","volume":"27","year":"2011"},{"abstractinfo":"制备了掺杂甲基红(质量分数1 %)向列液晶薄膜样品,测量了Ar+ 激光的透过率与样品厚度之间的关系,发现激光的偏振方向与液晶指向矢方向垂直时,透射率最大.选择Ar+ 激光作为写入光,重点利用二波耦合实验测量了一阶衍射效率随样品厚度、入射光夹角、两束入射光光强、两束入射光光强比的变化关系,实验发现当液晶薄膜样品厚度为32 μm,两束入射光夹角为2 °,两束入射光光强分别为80 mW/cm2且光强比为1∶1时具有最佳的全息存储实验条件.","authors":[{"authorName":"顾开宇","id":"b8c5e135-aa2c-4861-8d96-d4ac6ffe835b","originalAuthorName":"顾开宇"},{"authorName":"高洪跃","id":"ab3f4734-ffe6-47b0-a132-6f60b5adb34e","originalAuthorName":"高洪跃"},{"authorName":"周忠祥","id":"30121e64-650d-4a40-a6e4-71d6695c719a","originalAuthorName":"周忠祥"}],"doi":"10.3969/j.issn.1007-2780.2006.01.005","fpage":"19","id":"75b8dc71-b1a0-4cd2-88e0-4d793b0d8eb1","issue":"1","journal":{"abbrevTitle":"YJYXS","coverImgSrc":"journal/img/cover/YJYXS.jpg","id":"72","issnPpub":"1007-2780","publisherId":"YJYXS","title":"液晶与显示 "},"keywords":[{"id":"bec03a22-790f-46fb-8a01-6115cbcdd940","keyword":"向列液晶","originalKeyword":"向列液晶"},{"id":"b66320b9-a164-4149-a798-f55408efbf28","keyword":"甲基红","originalKeyword":"甲基红"},{"id":"953816c6-9e37-4f4d-b699-6131766f9993","keyword":"二波耦合","originalKeyword":"二波耦合"},{"id":"3a6f4815-b1ce-49aa-99d1-7a8259393570","keyword":"光折变效应","originalKeyword":"光折变效应"}],"language":"zh","publisherId":"yjyxs200601005","title":"无外场作用下掺甲基红向列液晶光折变特性实验研究","volume":"21","year":"2006"},{"abstractinfo":"热轧板带钢轧后冷却过程中,由于骤冷后表面与中心的温差导致轧件内部的热量传向表面,出现表面返红现象.对返红过程进行实验研究,实测了轧件在水冷后表层和内部温度的变化.用有限元法对不同规格轧件经历不同冷却条件下的返红情况进行模拟,分析钢板表面返红的原因,确定了发生返红的临界条件,得到了不同条件下返红引起的温升量和返红时间.结果表明,随着厚度和冷却速度的增大,水冷后心表温差增加,返红温升量增大,返红时间也增加.","authors":[{"authorName":"刘相华","id":"5b330799-0540-4211-9ed0-93bcf023b4f5","originalAuthorName":"刘相华"},{"authorName":"于明","id":"4ab84ce1-8799-43be-8d98-09229c4b5f1c","originalAuthorName":"于明"},{"authorName":"支颖","id":"a3127fa1-4242-4c75-af14-b4daab14c727","originalAuthorName":"支颖"},{"authorName":"谢海波","id":"e541b067-647a-451b-a1a1-8f4718aaf45e","originalAuthorName":"谢海波"},{"authorName":"喻海良","id":"26f43c3c-1066-4049-b09a-69ded554262e","originalAuthorName":"喻海良"}],"doi":"","fpage":"25","id":"abb06cca-6b52-46d2-ae16-62679f3351cf","issue":"10","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"bbcf51c8-7508-4f6d-9873-f446bb18f6e5","keyword":"板带钢","originalKeyword":"板带钢"},{"id":"3490b46a-e2dd-4b0d-90e5-d00c355db44b","keyword":"快速冷却","originalKeyword":"快速冷却"},{"id":"5b9ba47a-f301-4106-9bf0-fa451c25fccd","keyword":"表面返红","originalKeyword":"表面返红"}],"language":"zh","publisherId":"gtyjxb200810007","title":"板带钢快速冷却后表层返红现象","volume":"20","year":"2008"},{"abstractinfo":"热轧板带钢轧后冷却过程中,由于骤冷后表面与中心的温差导致轧件内部的热量传向表面,出现表面返红现象。对返红过程进行实验研究,实测了轧件在水冷后表层和内部温度的变化。用有限元法对不同规格轧件经历不同冷却条件下的返红情况进行模拟,分析钢板表面返红的原因,确定了发生返红的临界条件,得到了不同条件下返红引起的温升量和返红时间。结果表明,随着厚度和冷却速度的增大,水冷后心表温差增加,返红温升量增大,返红时间也增加。","authors":[{"authorName":"刘相华","id":"2f73aead-8e8f-4c7a-845e-46aeee6eb54d","originalAuthorName":"刘相华"},{"authorName":"于明","id":"d59a0a21-7742-442c-9bbf-16db9cbcc651","originalAuthorName":"于明"},{"authorName":"支颖","id":"c7297dde-e7b3-4e08-8acf-b9336d148655","originalAuthorName":"支颖"},{"authorName":"谢海波","id":"e3e8d43d-fad4-4fec-b5b5-71356c41646f","originalAuthorName":"谢海波"},{"authorName":"喻海良","id":"ac23104b-2524-4e84-aef7-e98c3f767183","originalAuthorName":"喻海良"}],"categoryName":"|","doi":"","fpage":"25","id":"ecccae4a-2843-4442-a85a-93e3535eda9f","issue":"10","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"936cdb69-17c1-4880-9fe8-a4633906efe7","keyword":"板带钢;快速冷却;表面返红","originalKeyword":"板带钢;快速冷却;表面返红"}],"language":"zh","publisherId":"1001-0963_2008_10_13","title":"板带钢快速冷却后表层返红现象","volume":"20","year":"2008"},{"abstractinfo":"","authors":[{"authorName":"光宇","id":"975f46c7-da6c-419a-9b20-4415ab5c7f29","originalAuthorName":"光宇"}],"doi":"10.3969/j.issn.1000-6826.2001.05.008","fpage":"11","id":"d0c2e0ac-8cb5-4fea-81f0-63da2530cdc9","issue":"5","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"9e8bbac8-103b-4868-ad5d-5d8445d9bb75","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj200105008","title":"坦克家族特种兵","volume":"","year":"2001"},{"abstractinfo":"综述了对红柱石莫来石化及其烧结行为的研究,探讨了优化红柱石基耐火材料制备工艺的途径.","authors":[{"authorName":"李柳生","id":"95626a9a-ce11-4d94-8211-5b7a71fcc68f","originalAuthorName":"李柳生"},{"authorName":"平增福","id":"9d520522-43f4-49bb-a1b8-56561b0e33d7","originalAuthorName":"平增福"}],"doi":"10.3969/j.issn.1001-1625.2006.01.010","fpage":"34","id":"11bac563-095d-4b26-a455-8716315e9acb","issue":"1","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"b643aca9-27d6-4def-9f11-79aa7246099d","keyword":"红柱石","originalKeyword":"红柱石"},{"id":"9dd6eb20-c60f-493d-bb8c-44869f592f3e","keyword":"莫来石化","originalKeyword":"莫来石化"},{"id":"fc41d258-add7-4774-85c8-bee4ef069309","keyword":"烧结","originalKeyword":"烧结"}],"language":"zh","publisherId":"gsytb200601010","title":"红柱石的莫来石化","volume":"25","year":"2006"},{"abstractinfo":"红古铜工艺是仿古技术之一,是用电镀、染色和机械打磨而成的.介绍了采用低氰工艺预镀底层.锌合金压铸件在预镀铜后,焦磷酸铜镀液加厚镀铜;而铁件预镀铜后,常温硫酸铜镀液加厚镀铜,打磨定型,涂漆封膜.","authors":[{"authorName":"李庆恩","id":"6108cb69-bef1-4264-ae80-141267077305","originalAuthorName":"李庆恩"}],"doi":"10.3969/j.issn.1001-3849.2009.08.008","fpage":"28","id":"998956af-0bc7-4ed2-94b9-342e8fc9b5c5","issue":"8","journal":{"abbrevTitle":"DDYJS","coverImgSrc":"journal/img/cover/DDYJS.jpg","id":"20","issnPpub":"1001-3849","publisherId":"DDYJS","title":"电镀与精饰 "},"keywords":[{"id":"770ba93e-41a5-4015-9faf-f2987e7394a2","keyword":"红古铜","originalKeyword":"红古铜"},{"id":"8ee90f77-d375-47e7-ae25-f15abcedd5ec","keyword":"着黑色","originalKeyword":"着黑色"},{"id":"9949c828-fbdb-4214-80b9-1df5201cd5b8","keyword":"低氰镀液镀铜","originalKeyword":"低氰镀液镀铜"},{"id":"e1d2be2e-140a-45d7-99c1-61e57a610ce7","keyword":"打磨定型","originalKeyword":"打磨定型"}],"language":"zh","publisherId":"ddjs200908008","title":"仿红古铜表面加工工艺","volume":"31","year":"2009"},{"abstractinfo":"以Zn(NO3)2和曙红的混合溶液为沉积液,采用阴极电化学沉积法在ITO导电玻璃上制备了纳米多孔ZnO/曙红复合膜.考察了电化学预处理过程和曙红浓度对薄膜晶体结构、微观形貌和光学性能的影响.结果表明,引入短时间的电化学预处理过程能提高复合薄膜中ZnO的结晶质量,并诱导ZnO沿c轴定向生长.随着电沉积液中染料浓度的增大,所得薄膜的结晶质量下降,薄膜由六角晶颗粒逐渐向纳米多孔结构转变.当沉积液中曙红浓度为50μmol/L 时所得复合薄膜具有最大膜厚,装载的曙红量最高.以该复合膜为光阳极制作了太阳能电池原型器件,其开路电压为0.49V,短路电流为0.67mA/cm2,总光电转换效率为0.105%.
","authors":[{"authorName":"甘小燕","id":"8050054d-7490-45c1-acb9-5491b1d63cea","originalAuthorName":"甘小燕"},{"authorName":"李效民","id":"5da665eb-e6d5-4160-96c6-4e3cfc9e565b","originalAuthorName":"李效民"},{"authorName":"高相东","id":"aa8af556-21d2-45a1-b853-d646fa03b2dc","originalAuthorName":"高相东"},{"authorName":"于伟东","id":"adc3cd8f-6dec-4570-bf53-76d16f7547db","originalAuthorName":"于伟东"},{"authorName":"诸葛福伟","id":"f78c4b3b-1231-4e9d-96d6-65f0d1f76215","originalAuthorName":"诸葛福伟"}],"categoryName":"|","doi":"10.3724/SP.J.1077.2009.00073","fpage":"73","id":"7c5477a0-66ec-462c-90e7-e334bef120d4","issue":"1","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"c35b98ff-18e1-4ae0-a1ee-73721e678d83","keyword":"ZnO","originalKeyword":"ZnO"},{"id":"993647dd-a73c-4425-af60-10c99eedfa16","keyword":" Eosin Y","originalKeyword":" Eosin Y"},{"id":"df5f1990-5232-4dfa-b0a1-2d2fdde97684","keyword":" electrodeposition","originalKeyword":" electrodeposition"},{"id":"d7a77995-1cfb-40b7-b070-482112687348","keyword":" dye-sensitised solar cell","originalKeyword":" dye-sensitised solar cell"}],"language":"zh","publisherId":"1000-324X_2009_1_12","title":"电化学沉积法制备纳米多孔ZnO/曙红复合薄膜","volume":"24","year":"2009"},{"abstractinfo":"以Zn(NO3)2和曙红的混合溶液为沉积液,采用阴极电化学沉积法在ITO导电玻璃上制备了纳米多孔ZnO/曙红复合膜.考察了电化学预处理过程和曙红浓度对薄膜晶体结构、微观形貌和光学性能的影响.结果表明,引入短时间的电化学预处理过程能提高复合薄膜中ZnO的结晶质量,并诱导ZnO沿c轴定向生长.随着电沉积液中染料浓度的增大,所得薄膜的结晶质量下降,薄膜由六角晶颗粒逐渐向纳米多孔结构转变.当沉积液中曙红浓度为50μmol/L 时所得复合薄膜具有最大膜厚,装载的曙红量最高.以该复合膜为光阳极制作了太阳能电池原型器件,其开路电压为0.49V,短路电流为0.67mA/cm2,总光电转换效率为0.105%.","authors":[{"authorName":"甘小燕","id":"e224fb9b-f61a-44fb-85b3-28536e1661c0","originalAuthorName":"甘小燕"},{"authorName":"李效民","id":"ec7f0405-dfcc-4588-83b0-1980dd3c8803","originalAuthorName":"李效民"},{"authorName":"高相东","id":"86b9a57b-44fd-4107-9bb4-d964a723813a","originalAuthorName":"高相东"},{"authorName":"于伟东","id":"cb77f0d4-d62e-4c26-baca-f78dabd26685","originalAuthorName":"于伟东"},{"authorName":"诸葛福伟","id":"ab2d9711-c91f-44f1-b1a7-975ca92f0e49","originalAuthorName":"诸葛福伟"}],"doi":"","fpage":"73","id":"52b9ada3-aa72-4234-9f3c-7a054ab3b572","issue":"1","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"9420b651-b558-4c64-85b3-c461256fb0be","keyword":"ZnO","originalKeyword":"ZnO"},{"id":"be15765d-4a46-49f0-afeb-980ae194053c","keyword":"曙红","originalKeyword":"曙红"},{"id":"b9285961-2798-4354-985a-f3216b821f65","keyword":"电化学沉积","originalKeyword":"电化学沉积"},{"id":"0b8e4fc4-e8f6-44f4-8501-1b765f58f81e","keyword":"染料敏化太阳能电池","originalKeyword":"染料敏化太阳能电池"}],"language":"zh","publisherId":"wjclxb200901016","title":"电化学沉积法制备纳米多孔ZnO/曙红复合薄膜","volume":"24","year":"2009"},{"abstractinfo":"为了优化红柱石基耐火材料的生产工艺参数,寻求生产热风炉用优质红柱石砖的最佳工艺路径,研究了红柱石粗颗粒预烧温度对红柱石基耐火材料物理性能的影响,并探讨了影响机制。首先将南非红柱石粗颗粒(4~1 mm)分别在1300、1400、1500、1600℃下预烧3 h,再与红柱石的中颗粒(≤1 mm)和细粉(≤0.088 mm)以及烧结氧化铝粉(≤0.044 mm)和结合黏土进行配料制样后,于1500℃保温3 h 烧成,然后检测试样的体积密度、显气孔率、耐压强度、烧成线变化及1400和1550℃下的压蠕变率(载荷0.2 MPa,保温时间50 h),并采用XRD 分析试样压蠕变试验前后的物相组成。结果表明:经1400℃预烧的红柱石粗颗粒在试样烧成过程中产生的体积收缩减弱了二次莫来石化反应的膨胀效应,可使试样获得较好的物理性能;预烧红柱石粗颗粒保留的未平衡状态在材料高温压蠕变过程中将继续向平衡态发展,期间产生的膨胀效应有效地抵抗了压缩蠕变。可见,在本试验条件下,将红柱石粗颗粒于1400℃左右预烧后使用,可以有效改善红柱石基耐火材料的物理性能。","authors":[{"authorName":"李柳生","id":"7b8523ad-af48-4bb8-b4a7-b0766949956f","originalAuthorName":"李柳生"},{"authorName":"廖桂华","id":"d5efe789-679e-4495-b669-89d4012441ce","originalAuthorName":"廖桂华"},{"authorName":"徐国辉","id":"ec7e8e36-41b4-46a9-835e-07821e715330","originalAuthorName":"徐国辉"},{"authorName":"李坤鹏","id":"cfec6a5a-f837-4cbe-8388-130c8535a7a2","originalAuthorName":"李坤鹏"},{"authorName":"王青峰","id":"64f7a041-9f80-49e4-8ba9-e40f4f1283c2","originalAuthorName":"王青峰"},{"authorName":"叶国田","id":"c24f9950-2f58-4966-8932-ea470ba22b23","originalAuthorName":"叶国田"}],"doi":"10.3969/j.issn.1001-1935.2016.05.001","fpage":"321","id":"ae9be1fc-348f-4c0d-a083-7f552b4e20ec","issue":"5","journal":{"abbrevTitle":"NHCL","coverImgSrc":"journal/img/cover/NHCL.jpg","id":"55","issnPpub":"1001-1935","publisherId":"NHCL","title":"耐火材料 "},"keywords":[{"id":"04e7a363-b114-4f83-a817-1598d9764e9c","keyword":"红柱石颗粒","originalKeyword":"红柱石颗粒"},{"id":"43a243b9-2f2a-4bcd-ae98-9b54d1216b46","keyword":"预烧温度","originalKeyword":"预烧温度"},{"id":"02272832-31e3-4fa2-a4f1-60a57e335433","keyword":"莫来石化","originalKeyword":"莫来石化"},{"id":"bf1762f6-2f68-465c-b50c-364b1af9463b","keyword":"抗蠕变性","originalKeyword":"抗蠕变性"}],"language":"zh","publisherId":"nhcl201605001","title":"红柱石粗颗粒预烧温度对红柱石基耐火材料性能的影响","volume":"50","year":"2016"}],"totalpage":906,"totalrecord":9054}